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GCMS analysis results for sample AE10522, May 2002

Machine-extracted title · confidence 100%

GCMS analytical report for sample AE10522 showing unknown compounds and surrogate recovery data from May 22, 2002.

NYC-WTC_000045386–000045395

Folder label: “GCMS X 5/2/02 A 5/12/02

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Scanned page image, NYC-WTC_000045394
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAY1002\10522.D Vial: 45 Acq On : 12 May 2002 8:58 am Operator: Sample : gc/ms scan 5/2 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 25.68 0.47 ug/1 62811 Phenanthrene-dl0 25.55

Hit# of /5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 72 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 Antipyrine 188 C11H12N20 000060-80-0 40 4 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 28 Abundance Scan 2252 (25.678 min): 10522.D (-) m/z 188.15 100.00% 108

5000

94 V "dT 80 25.40 25.60 25.80 26.00 42 52 66 . 158 132 — rr[ in i | I i r i [ f / i j TTTTp ! I I i | i_i H [ i i i i [ I i i । r 1111 ' i'''' । 4 m/z 94.10 21.24% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 25.40 25.60 25.80 26.00 m/z 189.15 14.24% 66 80 94 160 I I t | I I ! ! | ! ! I I | I I < ! [ I I I । । I I I I | I I 11 | r 0m " 1111111'111 I’T m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

25.40 25.60 25.80 26.00 5000 m/z 80.05 13.85%

80 94 160 66 ----- 1 ■11' TTTWETNI m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69177: Antipyrine 188 25,40 25.60 25.80 26.00 96 m/z 184.15 11.87% 77 5000 56 31 105 46 145 159 173 m/z—> ' 11 11 11 I '1 I TTT ----- - I . 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 JU 25.40 25.60 25.80 26.00

10522.D GCMS0510.M Thu May 16 16:20:06 2002 Page 2

NYC-WTC_000045394

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NYC-WTC_000045394Source: NYC Law Department, mirrored locally

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