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GCMS analysis results for sample AE09565, May 6 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09565 conducted on May 6, 2002.

NYC-WTC_000044349–000044359

Folder label: “GCMS X 4/23/02 A 4/26/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0102\9565.D Vial: 4 Acq On 1 May 2002 10:51 am Operator: Sample gc/ms scan 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 25.72 0.45 ug/1 30177 Phenanthrene-dl0 25.59 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-d10-/7 188 C14D10 001719-06-8 94 2 Phenanthrene-dl0' 188 C14D10 001517-22-2 91 3 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 40 4 Naphthalene, 1,7-dimethoxy-______ 18 8 C12H1202 005309-18-2 40 Abundance Scan 2257 (25.724 min): 9565. D (-) m/z 188.15 100.00% 188

5000 "1 I | ! I 4 pl I T i | I I i i । i i i i p 80 94 44 54 66 158 25.40 25.60 25.80 26.00 - 1111 | TT I H I I > ! | I I ' I I | I ! I ! | I | T-p-r m/Z 94.10 17.33%l m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

............ ) L 5000 1 1 1 1 ■ 1 i ■ 1 ' 1 i 25.40 25.60 25.80 26.00 m/z 189.15 15 .77% — 80 94 160 । 1OIPTPTTTTTTTT I 11 । ■ ■ ■ ■ । ■ - ■ ■ । ■ ■ ■ > । ■ ■ ■ ■ । ■ I 11' 1' 111 1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 1 I | । I 4 - i T i | I i I I [ I I I I—|"

25.40 25.60 25.80 26.00 5000 m/z 80.10 15.75%

80 94 160 .......................... 66 m/z-> 30 40 50 4 r 1 " i " " i " " i 60 70 80 90 100 110 120 130 140 150 160 170 180 190 1 | I I | i । i i । i i i > । r

. —— । । i । । । । 1 1 i । Abundance #69165: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 25.40 25.60 25.80 26.00 m/z 184.15 15.02%

5000 143 64 89 116 130 ill 158 170 — I I I I ‘ I I I 1 I > I I I I I I I I I I I I I I I 111 'I PI Ilf i । i ( j i । । i | I । । । j । r | / i 1 ‘1 11'11' i1 |rr T TH 1 TT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

9565.D GCMS0501.M Thu May 02 05:30:41 2002 Page 2

NYC-WTC_000044357

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NYC-WTC_000044357Source: NYC Law Department, mirrored locally

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