GCMS analysis results for sample AE09565, May 6 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAYO1O2\9565.D Vial: 4 Acq On 1 May 2002 10:51 am Operator: Sample gc/ms scan 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.19 16.74 ug/1 879359 1,4-Dichlorobenzene-d4 12.21

Hit# Of 5 'entative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 CH2=CHCHZC(O)OCH3 100 C5H802 003724-55-8 9 3 2,3-Butanedione, monooxime 101 C4H7NO2 000057-71-6 5 4 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 5 Abundance Scan 343 (8.185 min): 9565.D (-) m/ z 43.05 100.00% 43

5000 59

I I I I I I I I > I l—I I I I •" I I I I I I i 101 780 8.00 8.20 8.40 8.60 30| 5311 69 1 i 1 ' 1 •i 1 83 ' 1 i .0 m/z 59.10 43.84% m/z-> 10 20 30 40 50160 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 40

----- 5000 59 7.80 8.00 8.20 8.40 8.60 m/z 58.10 15.26% 27 101 49 — 83 1 ■ । 1 1 1 1 । m/z->_____ 10 20 1— 30 —40 50 । I ■ > 1 ■ । ■ ■ - - । ■' ■ ■ । I । 60 70 80 90 - 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.80 8.00 8.20 8.40 8.60 5000- m/z 101.15 13.52%

m/z-> 10 20 30 38 4 40 50 —.58—72 60 70 80 10* 90 100 100 110 Abundance #1607: 2,3-Butanedione, monooxime ■ । ' 1 ■ ' । 1 1 1 1 i ■ 1n"i ■ 1 1 1 i 1 1 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 7.32%

5000

15 101 ....... 1......... 30 38 1 ■ i 1 1 ■ 1 i ’ ' 1 1 1 1 1 1 1 1 1 51 58 ' I1-' 1 1 I ' ——————— 1 I I I I I I I I I I I I I I I I I I I ' I■ I ■I ■ I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9565.D GCMS0501.M Thu May 02 05:30:40 2002 Page 1

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