GCMS instrument log for sample AE09654, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAY2002\9654.D Vial: 12 Acq On : 20 May 2002 5:59 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.11 37.04 ug/1 1885470 1,4-Dichlorobenzene-d4 12.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4 - hydroxy-4-methyl - 116 C6H1202 000123-42-2 64 2 CH2=C: 2C(0)OCH3 100 C5H802 003724-55-8 9 3 Aceto: 58 C3H60. 000067-64-1 7 4 2,3-Butanedione, monooxime_________ 101 C4H7NO2 000057-71-6 7 Abundance Scan 335 (8.113 min): 9654. D (-) m/ z 43.05 100.00% 43

5000 59 7 101 7.80 8.00 8.20 8.40

m/z-> 0+ .......... 38 ; ■ ■

10 i ■ 1 ■ ■ i

20 ■ ' ' ■ i

30 ■ ■ f

40 11153.73 ■

50 60 69 70 77 83 80 90 fl 11 0 100 110 m/z 59.10 39.35% Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 —IPI-TT 59 7.80 8.00 8.20 8.40 m/z 58.10 16.16% 15 31 83 101 | Illi 1 ' I 1 1 1 1 I ' ' ' ' I ' 1 1 1 I 1 » ■ ■ l > — ——— m/z-> 10 20 30 40 50 60 70' 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 ■ ' ■ i ■ ' ' ■ i ‘ r ' ■ i 1 ■7 ' i ■ ■ ■ ' i

7.80 8.00 8.20 8.40 5000 m/Z 101.15 11.50%

........ 38, 1 i ■ ■ ■ ■ i ■ ' ■ ■ i ■ ■ ■ 1 r' 58 .1 72 1 00 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone 43 7.80 8.00 8.20 8.40 m/z 41.05 6.82% 5000 15 58 27 ----- ____________ j —___________ 1 ' ' i 1 1 1 । ■ 1 1 । ■ 1 1 1 । ■ * 1 ■ । 1 ■ * 1 । > ■ > > । > ■ ■ । ■ 1 ■ i ■ ■ ■ ■ । ' ' ■ ■ । ■ i m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

9654.D GCMS0520.M Tue May 21 11:38:18 2002 Page 1

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