GCMS instrument log for sample AE10064, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2002\10064.D Vial: 15 Acq On : 20 May 2002 8:56 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.11 31.17 ug/1 1830040 1,4-Dichlorobenzene-d4 12.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 64 2 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 3 2,3-But anedi one, monooxime 101 C4H7N02 000057-71-6 7 4 Acetone 58 C3H60 000067-64-1 7 Abundance 7 Scan 335 (8.112 min): 10064.D (-) m/ z 43.05 100.00%| 43

5000- 59

101 7.80 8.00 8.20 8.40

m/z-> O-TPPPPPP 10 20 30 38— 40 48 i 53 > ■

50 , ■ ■' f l f ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ ■ i 1

60 69 70 80 83 90 H 100 110 m/z 59.10 39.71% Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 m/z 58.10 16.51% 15 31 — 101 I - i 83 । ■ ■ । 100011 TH— i ■ ■ ■ ■ i ■ ' ■ ■ i ■ 1 i ■ 1 1 1 i 1 1 1 1 i 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 ■ 1 i ■ 114 i ' ' 1 ■i 7.80 8.00 8.20 8.40 5000 m/z 101.15 11.49%

miz—> 10 20 30 384 40 50 ... T.... 60 70 80 ■ i ■ ■ ■ ■ r1 1 ■ ' I 1 ' 1 ' i 1 90 100 100 110 Abundance #1607:2,3-Butanedione, monooxime 4)3 7.80 8.00 8.20 8.40 m/z 41.10 6.81%

5000

5 . 30,38, ' ' i ' 1 1 1 i 1 ■ ■ ' I 1 1 ' 1 r1 51 ' ' ‘ i ■ ' 58 1 1 i ■ ' ' ‘ i ' ■ 1 r i ■ ■ ■ ' i 1 1 1 ' 101 I' 1 1 1 I 1 _ ____________ _______ ■' । 1 1 ■1 i 11■ ' i ‘ ‘ i 1 ■ ■ ■ । m/z—> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

10064.D GCMS0520.M Tue May 21 11:37:55 2002 Page 1

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