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GCMS analysis results for sample AE03914, Mar 18 2002

Machine-extracted title · confidence 50%

Laboratory report documenting GCMS analysis of sample AE03914 for unknown compounds on March 18, 2002.

NYC-WTC_000038352–000038363

Folder label: “GCMS X 2/22/02 A 2/24/02

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NYC 9/11 Public Portal Document Library aearen compound Keporc

Data File : C:\HPCHEM\1\DATA\FEB2102\3914.D Vial: 76 Acq On : 24 Feb 2002 8:48 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,6-Dioxacyclododecane- 7,12-di Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

21.18 0.35 ug/1 33768 Acenaphthene-dl0 21.29

Hit# of 5 Tentative ID MW Mol Form' CAS# Qual

1 1,6-Dioxacyclododecane-7,12-dione 200 C10H16O4 000777-95-7 33 2 2H-Pyran, 3,4-dihydro- 84 C5H80 000110-87-2 32 3 Cyclopentanone 84 C5H80 000120-92-3 27 4 Cyclooctane 112 C8H16 000292-64-8 22 'Abundance Scan 1757 (21.176 min): 3914.D (-) m/ z 55.00 ’ 100.00% 55

5000- 84 41 . 100 111 129 TI X IT 156 20.80 21.00 21.20 21.40 21.60

m/z-> ■ l "' 'I" ■ ■ 111 i" " TH i -Ll 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 83.95 44.11% Abundance #22852: 1,6-Dioxacyclododecane-7,12-dione I 55 i i 5000 - 27 84 IT 42 20.80 21.00 21.20 21.40 21.60 100 71 129 m/z 56.00 27.06% 111

m/z-> TT 11' "I J, I . ■ i " ■ ■ i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 X ■rrpn I • •' ’ I 172 n+rr i *' “ i 200 TTTTT

'Abundance #62716: 2H-Pyran, 3.4-dihydro- 55 27 TI V 20.80 21.00 21.20 21.40 21.60 5000 84 m/ z 41.05 25.37% . 39 1

TT 69 11 ‘b 11 ’1" I' •1' I i... ;.. _ I" " 11"11 ‘1 ‘1111' ’ I •" ' I " " I " "11 ‘’ I" " I " " I i • ’4' i m/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #558: Cyclopentanone ‘id A TTI.T V 55 20.80 21.00 21.20 21.40 21.60 m/z 111.00 25.07% 5000 84 27 42 67 ' i' H I11''I i • •111" " r •" i'1 ‘ • r •" i p-rrrp-rrq- Tilr T-r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.80 21.00 21.20 21.40 21.60

3914.D GCMS0208.M Wed Mar 13 11:36:08 2002 Page 3

NYC-WTC_000038361

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NYC-WTC_000038361Source: NYC Law Department, mirrored locally

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