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GCMS analysis results for sample AE03914, Mar 18 2002

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Laboratory report documenting GCMS analysis of sample AE03914 for unknown compounds on March 18, 2002.

NYC-WTC_000038352–000038363

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038360
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Data File : C:\HPCHEM\1\DATA\FEB21O2\3914.D Vial: 76 Acq On : 24 Feb 2002 8:48 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise .Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method.: C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 3-Hydroxy-3-methyl-2-butanone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

9.27 0.28 ug/1 19541 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW Mol Form' CAS# Qual

• 1 3-Hydroxy-3-methyl-2-butanone 102 C5H10O2 000115-22-0 45 2 Butanand.de 87 C4H9NO 000541-35-5 38 3 Acetamide 59 C2H5NO 000060-35-544 4 Butanal , oxime 87 C4H9NO 000110-69-0 4 Abundance Scan 460 (9.269 min): 3914.D (-) m/ z 0" 59

5000- 43

69 84 151 9.00 9.20 9.40 9.60 ■ i > ■ • • i ■ - L III 'I'+I' j| m/ Z 42.95 45.25% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 'Abundance #63478: 3-Hydroxy-3-methyl-2-butanone 59

5000 31 43 I AAA 9.00 9.20 9.40 9.60 m/z 41.05 21.11% — ,. „.. 87. A. ,.. —.. m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62880: Butanamide 44 59

9.00 9.20 9.40 9.60 5000- m/z 69.00 10.74% 27 72 87 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 'Abundance #103: Acetamide 59 9.00 9.20 9.40 9.60 44 m/ z 150.90 9.76% 5000

m/z-> —l 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 9.00 9.20 9.40 9.60

3914.D GCMS0208.M Wed Mar 13 11:36:03 2002 Page 2

NYC-WTC_000038360

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NYC-WTC_000038360Source: NYC Law Department, mirrored locally

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