GCMS analysis results, sample AE05233, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5233.D Vial: 44 Acq On : 31 Mar 2002 11:38 am Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,6-Dioxacyclododecane-7,12-di Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

21.08 0.61 ug/1 102540 Acenaphthene-dl0 21.19

Hit# of Tentative ID 5 MW MolForm CAS# Qual 1 1,6-Dio:^cyclododecane-7,12-dione 200 C10H16O4 000777-95-7 37 2 Cyclopentanone 84 C5H8O 000120-92-3 22 3 Ethyl ^-decanoate 198 C12H22O2 000000-00-0 14 4 2-Hex^e 84 C6H12 000592-43-8 10 Abundance Scan 1746 (21.076 m'in); 52^LD0’ I K

5000 84

41 100 111 129 I WrTTTrjUrrXv Il 141 172 182 -,-jL..... 20.80 21.00 21.20 21.40 m/z 84.00 47.78% 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 'Abundance #22852:1,6-Dioxacyclododecane-7,i 2-dione ■ 55 i

5000 27 84 42 100 20.80 21.00 21.20 21.40 71 129 m/z 111.00 30.10% H pr . I 172 I'' " I 200 '' I'' (ti/z->____ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #5.58: Cyclopei'tanone 55

I ....... M....... 20.80 21.00 21.20 21.40 5000 84 m/ z 56.00 25.82% 27 1 42 67 I (nfe-->__ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #22384: Ethyl 9-decanoate 5 S8. 20.80 21.00 21.20 21.40 69 m/z 129.00 25.13% 5000 ■ loSio 123 ^35 152 l! 198 rrrp- ' I'' " I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.80 21.00 21.20 21.40

5233.D GCMS0308.M Wed Apr 03 13:57:25 2002 Page 3

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