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GCMS analysis results for sample AD24430, Nov 2001

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Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AD24430 conducted on November 7, 2001.

NYC-WTC_000068366–000068376

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24430.D Vial: 8 Acq On : 2 Nov 2001 9:52 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Acetic acid, 1,1-dimethylethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.70 0.50 ug/1 73456 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acdxJ, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 50 2 2-Pentapone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 42 3 Oxirape, (propoxymethyl)- 116 C6H12O2 003126-95-2 33 4 2-P9<K:anone, 5-(2-propynyloxy) - 140 C8H12O2 055702-70-0 17 4bundan^ Scan 289 (7.700 min): 24430.D (-) m7z 42.95 100.00% 40

5000 59

101 7.40 7.60 7.80 8.00 ............. |iill|i.i,| 83 pTTTTm+rU m/z 59.05 48.37%

L TTfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #64325: Acetic acid, 1,1-dimethylethyl ester 4(3

57 5000 7.40 7.60 7.80 8.00 101 m/z 100.95 18.98% 89 I " J ■ “I "' ‘ I' +t I,,>11,,.. I. >, 11 nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 ^bundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 4(3

7.60 7.80 8.00 5000 m/z 58.05 14.63% 59

27 101 83 ..... I I “'' I “'' I" " 1 .. . mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #3277: Oxirane, (propoxymethyl)- 40 ' '7.^ 7.60 7.80 8.00 57 m/z 42.05 7.84% 31 5000

I " " I ■ " • 1 "I' I ‘ ‘ I I I 87 n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 7-40 7.60 7.a0 8.00

24430.D NP103001.M Tue Nov 06 08:06:56 2001 Page 1

NYC-WTC_000068374

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NYC-WTC_000068374Source: NYC Law Department, mirrored locally

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