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← Document results/DEP Box 60/508 GCMS Scan X 10/11/01 An 11/2/01
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GCMS analysis results for sample AD24430, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AD24430 conducted on November 7, 2001.

NYC-WTC_000068366–000068376

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068375
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24430.D Vial: 8 Acq On : 2 Nov 2001 9:52 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.53 ug/1 76511 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 ihtative ID MW MolForm CAS# Qual 1 1,4-Dich]^obenzene-d4 150 C6C12D4 003855-82-1 50 2 BenzeneTzl,2,3,4-d4-, 5,6-di chloro- 150 C6C12D4 002199-69-1 32 3 Benzeiumine, 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 22 4 Benz famine, 2-methyl-5-nitro- 152 C7H8N2O2 000099-55-8 14 *Mjundance t Scan 711 (11,574 tnin): 24430.D (-) m/z 149.90 100.00% 100

5000 115 52 78 ‘H’ T 1120 11.40 11.ro 11.80 12.00

■nJz-> 30 40 50 60 Ulr 487 4^ m/z 151.90 70 80 90 100 110 120 130 140 150 160 64.71% Abundance #9593:1,4-D!chiorobenzene-d4 1$0

5000 115 . , . . ■ . I , . . r, . 1 . yI . I I 1 I

78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 . 36.32%

nft-> 30 35 40 50 UUr 60 70 80 90 100 110 120 130 140 150 160 1''' ‘ I

Sundance #9592: Benzene-1,2,3,4-d4-, 5,6-<iichloro- 100 11 ‘l'l.^‘ Vl!^' 'I'tso' ‘iZOD 115 5000- 52 78 m/z 78.05 . 20.51%

87

nfe-> 30 35 I 40 50 ' I • • • ' I ■ ■ 60 I H I I ‘ I ‘ 70 80 90 100 110 120 130 A I ‘ ‘ • I 140 150 160 ^bundance #10129: Benzenamine, 2-methyI-4-nitro- 77 106 1$2 i‘i .^' '11'40' 'i7.ro '1'1'so' '1'2'00 m/z 52.00 16.38%

5000 51 94 66 '' I ‘ ‘ ‘ ‘ I ‘' I ‘ nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24430.D NP103001.M Tue Nov 06 08:06:58 2001 Page 2

NYC-WTC_000068375

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NYC-WTC_000068375Source: NYC Law Department, mirrored locally

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