GC/MS analysis results for sample AD23502, Oct 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1601\23502.D Vial: 10 Acq On : 16 Oct 2001 11:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.53 ug/1 54510 1,4-Dichlorobenzene-d4 11.76

. Hit# of 5 ntative ID MW MolForm CAS# Qual

1 1,4-Dich]^obenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzo [b]z1^iophene-4-ol 150 C8H6OS 003610-02-4 23 3 Benzen^ine, 2-methyl-4-nitro- 152 C7H8N2O2I 000099-52-5 14 4 Benz^e-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 Abundance / Scan 717 (11.626 min): 23502.D (-) pm/z 149.90 100.00% 1!i0 I 5000 115 52 78 40 11.20 11.40 11.60 11.80 12.00 111' I'' I II ......... ill,..”............ '' I ' ''' I m/z 151.90 65.19% •n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

88551 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 31.67% 35 87 - Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9645: Benzo[b]thiophene-4-ol -1!i0.

121 11.20 11.40 11.60 11.80 12.00 5551 “m/z 78.05 18.34%

Tife-> Abundance 30 40 50 60 70 80 90 ... 100 110 120 130 140 -150 160 #10129: Benzenamine, 2-methyl-4-nitro- 77 106 4

i:'2. a ■1.1.20, 11.40-11.60 11,80 -12.00 .m/z- -52.00 15-.^2.8%

5000 51 —94____ 66 ' I ' ' I ' ' ' ' I ' I ' ' ' « I ' ' ' ' I '' I ’ ‘n/z--> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23502.D NP091101.M Thu Oct 18 10:24:48 2001 Page 4

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