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GC/MS analysis results for sample AD23502, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23502 conducted on October 19, 2001.

NYC-WTC_000088880–000088904

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088891
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23502.D Vial: 10 Acq On : 16 Oct 2001 11:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 5 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.51 3.94 ug/1 463042 Chrysene-dl2 33.13

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hex^ecanoate 312 C2 0H40O2: 000000-00-0 32 2 Oxiraney^ ,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 32 3 CyclofaXtane, 1,1-dimethyl-2-octyl- 196 Ci4H28 062338-30-1 27 4 1-He^ne, 2-methyl- _____________ 98 C7H14 006094-02-6 27 “Sundance/ Scan 2665 (29.509 min): 23502.D (-) pm7z 56.00 100.00% 53 *

5000 4' 73 129 257 . ..p..,,. n/z-> Abundance 20 40 60 1^157171185^99213 312 pTTp- I-'-... .. I 80 100 120 140 160 180 200 220 240 260 280 300 #44549: Butyl hexadecanoate 239

Jr X _29,20_294g_2a60_^a80__ m/z 56795 48.02%

53

5000 258 T-T-p-r ....... 29.20 29.40 29.60 29.80 73 240 312 m/z 43765 40.94% 129

■nZz-> 20 40 Ji 60 101 I 'll ' I ' ' ' ' I ' ' ' I ‘ ' I ' ' ' ' I ' ' ‘ ' I 'I' 80 100 120 140 160 180 200 220 240 260 280 300 I ' ' ' ' I "T

Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 53 41 J'..... PUJ." 29.20 29.40 29.60 29.80 5000 m/z 41.05 39.11% 73 113128 I .... I . Ti . I . . 1-. I ■p-rT-Tp-TT-T-pT-TTp-T-TT-p-rT^ Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- . I ,^-r i pp' ■*' I f-T'-r 53 29.20 .29.40 _ 29.60, 29.80 m7z 73-.-00 29.76%

5000

70

Ti/z-> 27

20 |\ 40 Vu 60 80 97 111125140 168 1-11igg ...... ...........................................................

100 120 140 160 180 200 220 240 260 280 300 111 I • ' ' ' J ' * ' I I I I I I I . I I . I I 1 I I I ' ' I ' ‘ ' I 'X I I ' 1 n I I I

29.20 29.40 29.60 29.80

23502.D NP091101.M Thu Oct 18 10:24:50 2001 Page 5

NYC-WTC_000088891

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NYC-WTC_000088891Source: NYC Law Department, mirrored locally

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