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GC/MS analysis results for sample AD23502, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23502 conducted on October 19, 2001.

NYC-WTC_000088880–000088904

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088892
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NYC 9/11 Public Portal Document

'iribrary Search Compouhd Report Data File : C:\HPCHEM\1\DATA\OCT1601\23502.D Vial; 10 Acq On : 16 Oct 2001 11:02 pm Operator; 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L *********************************************************************. Peak Number 6 Hexatriacontane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 29.62 0.92 ug/1 107671 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Octadecane 254 C18H38 000593-45-3 91 3 Heptadecane 240 C17H36 000629-78-7 9T 4 Tetracosane ___________________________ 338 C24H50 000646-31-1 90 Abundance Scan 2677 (29.619 min): 23502.D (-) m/z 57700 107700% 57 43 71

5000 85

99 113 29.20 29.40 29.60 29.80 30.00 y-rJ 1,1 127 141 155 169 207 “mTz 47700 75.09% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #74636: Hexatriacontane 43 57

71 5000 85 29.20 29.40 29.60 29.80 30.00 m/z 71.00 67.62% 155 169 183 197 211 * nnfe-> 40 60 80 100 120 140 160 180 200 220 240 /Abundance #71560: Octadecane 43 5 7 I [j \ /\ 71 29.20 29.40 29.60 29.80 30.00 5000 85 “m/z 85.05 46.23%

99 113

tnfe-> ' 'I' 40I 60 80 X100 127 141 169 183 197 210 I ' ' ' ’ I ' ’ ' ' I ' ' ' ' I ' ‘ 120 140 160 180 ' I . I I • I . . . . I « «' 200 220 240 I

Abundance #71193: Heptadecane ..... />........... , , 57 29.20 29.40 29.60 29.80 30.00 „m/.z__ 41.05 77770% 71 5000 85

99 , „l 141 155 169 210 240 ' ' I ' ' ' ' I ' ' ' 'I ' ' I ' I ' ' ' ' I' ' ' ' ■' I ' '■ ' ' I ' ‘ ' I ' ' ' ' I ‘ ' I ' ' ' ' I ' 'I ’ m/z-> 40 60 80 100 120 140 160 180 200 220 240 29.20 29.40 29.60 29.80 30.00

23502.D NP091101.M Thu Oct 18 10:24:52 2001 Page 6

NYC-WTC_000088892

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NYC-WTC_000088892Source: NYC Law Department, mirrored locally

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