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GC/MS analysis results for sample AD22979, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22979 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087773–000087793

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0301\22979.D Vial: 5 Acq On : 3 Oct 2001 4:33 pm Operator: 209 GALOS Sample : gc/ms unknown - Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Butyl hexadecanoate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

29.54 1.58 ug/1 246086 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hexadi^anoate 312 C20H40O2 000000-00-0 59 2 1-Hexene, -methyl- ■98 C7H14 006094-02-6 27 3 Oxirane, /,3-bis(l-methylethyl)-, t 128 C8H16O 054644-32-5 23 4 Cyclopei^ anecarboxylic acid, 2-amin 129 C6H11NO2 040£82-05-l_17 Abundance /■' ................. Scan 2668 (29.537 mih)? 22979."D(-) ............... 5|6

5000 43 73 257 I 129

20 40 60 80 1 100 120 140 160 180 200 220 240 260 280 300 1' 199 TI 312 -t+tt 2020 2940 29,60 29.80 m/z 47.23% ■V Abundance #44549; Butyl hexadecanoate 5l6

5000 258 r-r-T^ 29.20 29.40 29.60 29.80 73 240 312 116129 m/z 43.0,5 37.37% I 101 J I 'I I ' 157171185 " I ' ' ' ' I ■ ■ i ■' I 1 ■ 214 ■ I ■ I 1 ■ I 1 ■ ■ I I 1 ' I ' ' ' ’ I ' I !m/z-> 20 40 60 100 120 140 160 180 200 220 240 260 280 300 Abundance #1354; 1-He.xene, 2-tnethyl- 56 T 29.20 29.40 29.60 29.80 5000 I m/z 41.05 34.11% 27 I L? 83 98 -p-n-rj- m/z-> 'Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #5067; Oxirane, 2.3-bis(1-methylethyl)-, trans- rn-p-rWTH- Ka 29.20 29.40 29.60 29.80 41 m/z 55.00 29.01% 5000 73

m/z-> 20 40 60 A 80 113128 I'''' I 100 120 140 160 180 200 220 240 260 280 300 TTTT-TyT-T-T-TYTTTTyT-TTTp--^^ tA-t 29.20 29.40 29.60 29.80

22979.D NP091101.M Tue Oct 09 09:54:18 2001 Page 3

NYC-WTC_000087782

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