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GC/MS analysis results for sample AD23079, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087794–000087816

Folder label: “GC/MS Scan 9/21/01

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Scanned page image, NYC-WTC_000087805
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NYC 9/11 Public Portal Document

Library Search Compound Report

'Data File C:\HPCHEM\1\DATA\OCT0 301\23079.D Vial: 6 Acq On 3 Oct 2001 5:32 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butyl hexadecanoate Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.54 1.17 ug/1 163085 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hexa>3ecanoate 312 C20H40O2 000000-00-0 25 2 Oxirane,/2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 23 3 1,3-He: nediol, 2-ethyl- 146 C8H18O2 000094-96-2 23 4 Cyclop :ntanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 17 Abundance Scanl668 (29.536 min): 23079.D (-) m/z 56.00 100.00% 5|6

5000 43 73 IL ^29 239 257 312 29.20 29.40 29.60 29.80 A I-.......... .. m/z 57.0.0 47.81% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Avbundance #44549; Butyl hexadecanoate s|5

5000 258 r*-r-r^ 29.20 29.40 29.60 29.80 73 240 312 m/z 43.0„5 36.71% 157171214 I I ' ' ' I ' ' ' ' I ' ' ' ' I ' ’ I - hi/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067; Oxirane. 2,3-bis(1-metliylett)yl)-, trarts- 56 41 29.20 29.40 29.60 29.80 5000 m/z 41.0.5 35.01% 73

i, ii T-p-m-p- 113 128 ■p-n-r-p-n-ry ' '' I'' '' I' ' '' I ‘' I'''' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #8882: 1,3-Hexanedioi, 2-ethyl- La ..A. I YI I V. r. I 5|6 29.20 29.40 29.60 29.80 m/z 73.00 28.92% 5000- 73

31 103 J ,, I ' I ‘‘ I I ' ' ‘ ' I ' ' ' ' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23079.D NP091101.M Tue Oct 09 09:57:51 2001 Page 5

NYC-WfC_0000‘87805

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NYC-WTC_000087805Source: NYC Law Department, mirrored locally

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