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GC/MS analysis results for sample AD23270, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.

NYC-WTC_000088346–000088371

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088357
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23270.D Vial: 18 Acq On : 12 Oct 2001 6:44 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* 'Peak Number 5 Butyl hexadecanoate Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 29.51 2.92 ug/1 310526 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl hexadecanoate 312 C20H40O2: 000000-00-0 32 2 Oxirane, 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 23 3 1,3^exanediol, 2-ethyl- 146 C8H18O2 000094-96-2 23 4 Cyc/opentanecarboxylic acid, 2-amin 129 C6H11NO2: 040482-05-1 17 ^undancf Scan 2665 (29.509 min): 23270. D (-) m/z 56700 100.00% 53

5000 4’ 73 257 129 239 JI. rirT.I 143157171185199213 29.20 29.40 29.60 29.80 312 I T I I I rj I V| . rt T ] 1' III I 'i I I I I I 11 I j I I I I I I I I I j rr^TT m/z 57.00 48.46% T1^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 55

553 258 LA TT-rr-t-n-Hr I ' I ■ 1 H I I I I 2920 2940 29.60 29.80 240 312 m/z , 7 116129 43.05 36.45% ..... ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 53 41 T*rT 29.20 29.40 29.60 29.80 5000- m/z 41.00 34.45% 73

113128 I' '' ' I' '' ' I' '' ' I' ''' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #8882:1,3-Hexanediol, 2-ethyl- 29.20 29.40 29.60 29.80 m/z 73.00 29.64%

5000 73

103 ,,| ' I ' ' I''' ' I' '' ' I' ''' I''' ' I' '' ' I' '' ' I''' ' I' ''' I' ''' I' '' ' I •n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23270.D NP091101.M Mon Oct 15 09:33:37 2001 Page 5

NYC-WTC_6o6o88357'

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NYC-WTC_000088357Source: NYC Law Department, mirrored locally

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