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GC/MS analysis results for sample AD23324, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.

NYC-WTC_000088316–000088345

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088328
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\OCT1201\23324.D Vial: 17 Acq On : 12 Oct 2001 5:46 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L **************************** *■* ***************************************

Peak Number 6 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.50 8.89 ug/1 1008200 Chrysene-dl2 33.12 Hit# of 5 Ti ■tative ID MW MolForm CAS# Qual . 1 Butyl hexa^ canoate 312 C20H40O2; 000000-00-0 64 2 1-Hexene,^ '2-methyl- 98 C7H14 006094-02-6 27 3 Oxirane 2,3-bis(1-methylethyl)t 128 C8H16O 054644-32-5 23 4 1,3-H^anediol, 2-ethyl-________________ 146 C8H18O2 000094-96-2 23 Abundance / Scan 2665 (29.504 min): 23324.D (-) m/z 56.00 100.00% 5^

5000 4' 73 129 257 312 _2a20_J940_29t0_^9;80___ ' 11111111P' I f Tf 11”,, IV11 f'l I I'l TI ,■ I'l 111111111111 i 1111,111111 'I,,, r,, I ,, I I .., I, -h-t m/z 57.00 45.78% TiZz-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #44549; Butyl hexadecanoate (1 55

5000 258 ....... . , / U 29.20 29.40 29.60 29.80

Tife-> Abundance 20 40 u 60 73 I 129 Il I •'^7171^^^ 80 100 120 140 160 180 200 220 240 260 280 300 #63261:1-Hexene, 2-methyl- 214 240 312 m/z 43700 37773%

53

29.20 29.40 29.60 29.80 41 m/z 41.00 3576^ 5000 27 70 98 I pTT-rpTT-rp-rTTpT-rrpT-rTpT-TTT-rTTn-p-rTTYTT-rT-pT-rTyrTTTpn-rT^^ '' I'''' I'' n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 5^ #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- T Ma 29.20 29.40 29.60 29.80 41 m/z 73.00 29733%

5000

73 113128 T-p-r-r-r-p- I'''' I'''' I I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' '-r I ' ' •n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23324.D NP091101.M Mon Oct 15 10:33:33 2001 Page 6

NYC-WTC_000088328

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NYC-WTC_000088328Source: NYC Law Department, mirrored locally

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