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GC/MS analysis results for sample AD22979, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22979 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087773–000087793

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0301\22979.D Vial: 5 Acq On 3 Oct 2001 4:33 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

11.64 0.52 ug/ 68800 1,4-Dichlorobenzene-d4 11.78

Hit# of 5 fentative ID MW MolForm CAS# Qual

1 l,4-Dich^robenzene-d4 150 C6C12D4 003855-82-1 78 2 Benzene^, 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 1,2,5-Trithiepane 152 C4H8S3 006576-93-8 10 42-Met^l-6-nitroaniline 152 C7H8N2O2 000570-24-1 10 Abundance Scan 719 (11.644 min): 22979.D (-) m/z 149.90 ,100.00% l40

5000 115 52 ^8 I ' ' ' ' I T 11.40 11.60 11.80 12.00

m/z~> 30 40 50 .... ....................... 60 70 80 90 100 110 rX120 130 140 150 160 m/z 151.90 , 64.90% Abundance #9593: 1,4-Dichlorobenzene-d4 I 150

5000 115 l\ 78 11.40 11.60 11.80 12.00 52 m/z 114.90 , 35.93% 35 rq-r-r-TT-p-r-r-r-p I hi/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance ^9592: Benzene-1.2.3.4-d4-, 5.6-dicbloro- 150

115 11.40 11.60 11.80 12.00 52 78 m/z 78.05 . 17.23% 5000

35 87 I!,I Tl/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10068: 1,2,5-Trithiepane 142 11.40 11.60 11.80 12.00 m/z 75.90 , 12.11% 5000 60 87 45 78 106 124

30 40 50 60 70 , ,1, 96.,, , I . ........ I............ L m/z-> 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

22979.D NP091101.M Tue Oct 09 09:54:13 2001 Page 2

NYC-WTC_000087781

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NYC-WTC_000087781Source: NYC Law Department, mirrored locally

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