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GC/MS analysis results for sample AD23500, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23500 conducted on October 19, 2001.

NYC-WTC_000088826–000088852

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088838
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NYC 9/11 Public Portal Document

Library Search Compound Report ' Data File : C:\HPCHEM\1\DATA\OCT1601\23500.D Vial: 8 Acq On : 16 Oct 2001 9:05 pm Operator: 209 GALOS, Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *************************************************************** * * * * * * Peak Number 6 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R’.T. 29.51 3.90 ug/1 392756 Chrysene-dl2 33.12

Hit# of 5 Tenrative ID MW MolForm CAS# Qual

1 Butyl hexad^anoate 312 C20H40O2; 000000-00-0 42 2 1-Hexene, -methyl- 98 C7H14 006094-02-6 27 3 Cyclobut^e, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 . 4 1,3-He30nediol, 2-ethyl-1^C8H18O2 000094-96-2 25 Abundance / Scan 2665 (29.508 min): 23500.D (-) m/z 56700 107700% 5

■ 5000 41 73 129 257 ..........................................................

Tife-> 20 40 60 ,4, 80 100 120 140 160 180 200 220 240 260 280 300 X., t,,,, Tp-n-rp-r+Ty 312 m/z 29,20 29,40 29,60 29,80 57700 48.32% Abundance #44549; Butyl hexadecanoate

5000 258 292g_J940_ja60_2a80^_ 240 312 m/z 43705 39700% 129 I?'’. I I 157171185 214 ' 'I '' " I' ' I' I'' " I'''' ' I'''' i'''' I mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance ___________ __#1354:.1rHexene,2-methyl- —_______ 55

41 29.20 29,40 29.60 29,80 T A 1

5000 m/z 41.05 37.15% 27

m/z-> 20 40 VA I

60 70

80 98 I ’''' r ' ’ ' I ' ‘ ' r ' ' ' I ' ' ' ' I ’ ' ’ 100 120 140 160 180 200 220 240 260 280 300 I

Abundance J^198^yclobut^e, 1,1 -dimethyl-2-octyl- .......... ,A ..... T5|B~“ — 29,20 29,40 . 29,60 29,80, _ m/z 73.00 29771%

5000

27 70 I t I, 97 111125140 168 195 I''' ‘ I'''' I' ‘ ’ r ''' r ’'' I ... m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 . 280 300 29,20 29,40 29,60 29,80

23500.D NP091101.M Thu Oct 18 10:17:52 2001 Page 6

NYC-Wtc_0b6088838 ‘

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NYC-WTC_000088838Source: NYC Law Department, mirrored locally

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