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GC/MS analysis results for sample AD23834, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23834 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089476–000089500

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089489
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NYC 9/11 Public Portal Document

Library Search Compound Report .Data File : C:\HPCHEM\1\DATA\OCT3001\23834.D Vial: 19 Acq On : 31 Oct 2001 8:04 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\l\METHODS\NP10i901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 1-Hexene, 2-methyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.45 2.45 ug/1 346981 Chrysene-dl2 33.05 Hit# of 5 ■Tentative ID MW MolForm CAS# Qual

1 1-Hexene, ^methyl- 98 C7H14 006094-02-6 27 2 Butyl hex^ecanoate 312 G20H40O2i 000000-00-0 ;25 3 1,3'-Hexa^diol, 2-ethyl- 146 C8H18O2 000094-96-2 25 4 Cyclobut^ne, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 25 Abundance J Scan 2659 (29.452 min): 23834.D (-) m/z 56.00 100.00% 53 I

5000 4 73 I 129 257 . . , . I , . 1 , I, -n . I , , , , Jj, J,I, JI n® I 1431571711851992P ^39 J 312 29.20 29.40 29.60 29.80 I'' '' I' I' . .... m/z 57.00 43.46% TT/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 A Abundance #1354:1 -Hexene. 2-methyl- 55

41 5000 29.20 29.40 29.60 29.80 27 m/z 43.05 3^723% I 70 98 I ’ ’ • « I” ’ • I •’" I '« ' • I ' ' ' • } • • ' ' I « « I ' • • I I • I ' I I tVz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate . 5J

29,20 29.40 29.60 29.80 253 258 m/z 41.00 32.79% 240 312 I ? ^29 ' '' I ' ' '' ' I '' ' ' I ‘ ' I ' ' ' tVz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #8882:1,3-Hexanediol, 2-ethyl- ___2a20_2a4g_^;6q_j9;8^ m/z 73.00 29.59% 5000

31 I I'''' I'''' I r ''' I ’''' r ''' I •I ' I ' * ' ’ 1 Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280'300 - 29.20 29,40 29.60 -29.80

23834.D NP103001.M Thu Nov 01 13:21:38 2001 Page 7

NYC-WTC_000089489

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NYC-WTC_000089489Source: NYC Law Department, mirrored locally

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