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GC/MS analysis results for sample AD23834, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23834 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089476–000089500

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089488
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT3001\23834.D Vial; 19 Acq On : 31 Oct 2001 8:04 am Operator;' 2 09 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.53 ug/1 78375 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 1,4-Dichlorc^nzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1, ^3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 27 3 4-Amino-22^hlorobenzonitrile 152 C7H5C1N2 020925-27-3 10 4 Benzalde^de, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Abundance Scan 711 (11,568 min): 23834,D (-) Tm/z 149.90 100700% 1!i0

5000

4, 7. 78 115 ..... -J\... 11,20 11,40 11,60 11,80 ,il 87, TT-p-t44Y'-vMiYr-r-rT-p-r-rTr7W+h-yTT-r-ryT-^^ ,1 m/z 151.90 . 60.14% ‘ ‘ I ' ■nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichloroben2ene-d4 1!i0

5000 115 78 11.20 11,40 11.60 11,80 52 m/z 114.90 43.27%

Ti/z-> 30 35 40 50 60 JUT, 70 80 90 100 110 120 130 140 150 160 1

Abundance #9592: Benzene-1,2,3.4-d4-, 5,6-clichloro- Y$0

115 11,20 11,40 11,60 11,80 5000- 52 78 m/z 78.05 19.55%

_ 87__

.„x.. 35 ---- '7. J,'777,.., ' I ' ' ' ' I ' T Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10110:4-Amino-2-chlorobenzonitrile 1$2 ~^H ,20~11~:40'~11,60~'1'1,80~~ "m/z 52700 15.89%

5000

117 125 .......................... ?... 76....... I i-p-ri-ryr-rrTyT-rrryr-ri-rYri-T-ry'TT-r-^^ I ' ' ' ' I .............n J . \ , 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11,20 11,40 11,60 11,80

23834.D NP103001.M Thu Nov 01 13:21:36 2001 Page 6

NYC-WTC_000089488

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NYC-WTC_000089488Source: NYC Law Department, mirrored locally

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