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GCMS analysis results, sample AD23915, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23915 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067635–000067650

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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Scanned page image, NYC-WTC_000067648
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23914.D vial: 12 Acq On : 18 Oct 2001 12:03 am Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C;\HPCHEM\1\METHODS\NP091101 .M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.52 ug/1 52826 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 T« tative ID MW MolForm CAS# Qual 1 1,4-Dichlor( ienzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-1, ,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 4-Amino- chlorobenzonitrile 152 C7H5C1N2i 020925-27-3 9 4 Bipheny !ne 152 C12H8 000259-79-0 9 Abundance Scan 716 (11.617 min): 23914.D (-) m/z 149.90 100.00% 1$0

5000 115 52 78 ...................... ................................ 40 11.y 11.40 11.60 11,80 1200 ........I'!''. .'I II I ’ * ‘ * I ''' ‘ I I ’ * ‘ ’ I m/z 151.90 68.35% mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1.4-Dichlorobenzene-d4 1!i0

5000 115 78 11^20 '1'1'40' '1'1 h'm '1'260' 52 m/z 115.00 40.38% 35 T ^14^ tnZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3.4-d4-, 5,6-dichloro- 1$0

115 11.^ 11,40 11.60 11,80 12.00 5000 52 78 ■m/z 78705 23.24%

35 87 I I 114^ I I I I ' ■ 1 ‘ ‘ ' I ’ ' ‘ ‘ I ‘ ‘ ' 1 ' ‘ ' I ‘ Tlfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 1«) Abundance #10110:4-Amino-2-ch!orobenzonitrile 1$2 11.:^ 11.40 11.60 11.80 12.00 "mTz 52.00 19.19% 5000

117 125 ..... I........ X....?,.... I, 1' ‘ ‘ I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00 1 '' ’' I TTj-rr I ' ‘ ‘ 1 ‘ ' I ' ' -ry-r-r-n-pr-r

23914.D NP101901.M Wed Oct 24 11:15:04 2001 Page 6 NYC-WTC_000067648

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NYC-WTC_000067648Source: NYC Law Department, mirrored locally

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