NYC 9/11 Public Portal Document
Library Search Confound Report
Data File : C:\HPCHEM\1\DATA\OCT1701\23914.D vial: 12
Acq On : 18 Oct 2001 12:03 am Operator: 209 GALOS
San^le : gc/ms unknown Inst : GC/MS 209
Mise Multiplrz 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 7 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
44.19 0.48 ug/1 40184 Perylene-dl2 37.23
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4,^7-tetrasilaoctane, 294 C10H30O2Si4 004342-25-0 28
2 1-Monolinolegylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 25
3 3-Isopropoxv<l,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 23
4 Silane, [ (X-methyl-1,3-propanediyl) 234 C10H2602Si2 056771-47-2 14
Abundance Scan 4264 (44.189 min): 23914.D (-) m/z 72.95 100.00%
73 221
A.,.
147
5000
281 355
191 429
'50' ' 160 '' IM
I XI SaSoaS"
200 400
I
450 500 550
43.80 44,00 44.20 44.40 44.60
m/z 221.05 82.76%
Abundance
A
#41682:3,6-Dioxa-2,4,5,7-tetrasiIaoctan8. 2.2,4,4,5,5.7,7-
147
73
5000
43!8o' 44'00 '44'^' 44'40 '44.60
191 m/z 147.00 75.67%
117 279
I Ti/z-> 50 100 150 200
I
1
IffiO 300
' I ■■3 ■ I
^‘460"^"^"^
Mjundance #58871; 1-Monolinoleoylglycerol trimethylsilyl ether
■73
I ' ' ' ' I
43.80 44,00 44,20 44.40 44.60
207
5(X)0 147 m/z 280.9534.72%
34 103
I 281
395
t . 482
Tlfe-> 50 100 150 200 300 350 400 " 500 ' 5OT
Mxjndance #60503:3-lsopropoxy-1,1,1.7.7.7-hexamethyl-3.5.5-tris(trim . 1 I I I I I • > . . 1 I I I . I I 1 . 1
73 43.80 44.00 44.20 44.40 44.60
m/z 355.05 33.95%
5000
147
221 281 327
‘ I ' ' ' ' I ‘ ' I ‘ ‘
11 T,
• I ‘ ‘ ‘ ' I ' ' ' ' H ' A I . . . . I ,
_______ 519 561
, I . , . , I , 1 , I I i , ■ 1 • • ■ • I ■ • • • I ■ I ■ . I > I ■ ■ I . ■
50 100 150 200 250 3(X) 350 4(X) 450 550 43.80 44.00 44.20 44.40 44.60
23914.D NP101901.M Wed Oct 24 11:15:07 2001 Page 7
NYC-WTC_000067649
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