GCMS analysis results, sample AD25460, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1501\25460.D Vial: 4 Acq On : 15 Nov 2001 7:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplrs 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 3,6-Dioxa-2.4,5,7-tetrasilaoct Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 39.63 0.76 ug/1 153661 Perylene-dl2 37.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-Dioxa-2,4,5,7-tetra^laoctane, 294 C10H3002Si4 004342-25-0 25 2 3-Isopropoxy-1,1,1,7,7/7-hexamethyl 576 C18H52O7Si7 071579-69-6 23 3 l,l,l,5,7,7,7-Heptam^yl-3,3-bis(t 444 C13H4005Si6 038147-00-1 17 4 2,6-Dimethyl-3,4-big<itrimethylsilyl 311 Cl5H29NO2Si2 000000-00-0 16 Abundance Scan 3767 (39.629 min): 25460.D (-) m/z73700100700% 7b 147 221 550 355 40 193.1 429 39.20 39.40 39.60 39.80 40.00 ' 7 ' ' ' ''i ' ■ ^'''1 ' ■ ' ■ I ■ ' > ■ I ' ' I ■ I > I m/z 147.00 72.03% Tlfe-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #41682:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4.4,5,5,7,7- 147 z;i

73 5000 39.20 39.40 39.60 39.80 40.00 191 m/z 221.05 58.96% 117 279

50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1.1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

39.20 39.40 39.60 39.80 40.00 5000 m/z 281.00 29.43% 147

I....... T., I. T, I .Tt I.,.. ■,., ■ ■, ■nfe-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5.7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 39.20 39.40 39.60 39.80 40.00 m/z 207.00 24.62% 147 5000 267 355 429 45 207 i II ij..... ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 39.20 39.40 39.60 39.80 40.00

25460.D NP103001.M Wed Nov 21 12:42:50 2001 Page 4

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