Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
NYC-WTC_000088905–000088934Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\OCT1601\23503.D Vial: 11 Acq On • : 17 Oct 2001 12:01 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1,00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 20 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 47.33 3.15 ug/1 300244 Perylene-dl2 37.23
Hit# of 5 Tent^ative ID MW MolForm CAS# Qual
1 3,6-Dioxa-^4,5,7-tetrasilaoctane, 294 C10H30O2Si4 004342-25-0 33 . 2 Trisiloxahe, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 27 3 3-Isop;i?6poxy-l, 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 25 4 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 12 Abundance Scan 4606 (47.329 min): 23503.D (-) m/z73700100.00% 73 147 221
5000 281 355
41 117 47.00 47.20 47.40 47.60 I 1 ' * ' I ' Wp-r T-ry ■f+t V ' ' ’ r' m/z 147.00 86.18% ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 ^bundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 2:>1
73 5000 47.00 47.20 47.40 47.60 191 m/z 221.05 74.01% 279 I ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet -73 147 47.00 47.20 47.40 47.60 5000 m/z 280.95 367^7% 281 45 369
Abundance IX 50 117 100 150 207 200 249 250 300 350 400 450 500 550 #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73_ —47.00 - 47.20~47.40 47.60 - m/z-355.05 " 28t33% 5000 147
221 281 327 415 519 561 50 100 150 200 250 300 350 ' 400 450 ' ■ ' 500 550 47.00 47.20 47.40 47.60
23503.D NP091101.M Thu Oct 18 10:29:24 2001 Page 20
NYC-WTC_000088931
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NYC-WTC_000087274
Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088207
Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088346
Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089418
Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088263
Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088853
Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088456
Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088556
Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088372
Laboratory report documenting GC/MS analysis of environmental sample AD23271 conducted on October 15, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089476
Laboratory report documenting GC/MS analysis of sample AD23834 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088316
Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
Filed in the same folder
NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
Filed in the same folder
NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
Filed in the same folder
NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
Filed in the same folder
NYC-WTC_000088753
Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.
Filed in the same folder