Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
NYC-WTC_000088905–000088934Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23503.D Vial: 11 Acq On . : 17 Oct 2001 12:01 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS' 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 19 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 44.20 4.01 ug/1 382247 Perylene-dl2 37.23
Hit# of 5 Tentative ID MW MolForm CAS# Qual;
1 3,6-Dioxa-^4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 43 ’ 2 Trisiloxa^afe, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 32 3 1,2-Ben?^nedicarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 27 4 Mercapjz^acetic acid, bis (trimethyls 236 C8H2 0O2SSi2 006398-62-5 17 Abundance Scan 4265 (44.198 min): 23503.D (-) m/z 73.00 100.00%! 70 147 221 5000- 281 355
41 96 I"' ‘I I"'*' I I " ' ' I "'''I \"I xX 43.80 44.00 44.20 44.40 44.60 m/z 147.00 837^9%
K mfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 1 I7 221
73 253 43.^ 44.00 44.20 44.40 44.60 191 m/z 221.05 65711% 117 279 1" " 1"'' ' I'"' I I ‘' r "' r "' I 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet .73 147 43.80 44,00 44,20 44.40 44.60. 223 ■m/z-^BlToy 32.35% 281 369 L 117 207 249 . , . .. I..... ' I" " I" " I" " I' " I" " I"'' I' ’'' I" " I" " r'"' I"' 'T' • " I • I . . I M I . j . . . , . I . . I . M . I H I i I •n/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e 1 7 43.80 44.00 44.20 44.40 44.60 m/z—355-.-05 27.02% 73 5000
45 295
I I ‘I , 119 . 193 221 [ 4TTTTTTTT;4;rfTfAnWTrpTTTprrrfTTTiTrrrrpTTTpTrtpTiTpyrTT^^ ■n/z-> 40 60 80 100120140160180200220240260280300320340360380400420 43.80 44.00 44.20 44.40 44.60
23503.D NP091101.M Thu Oct 18 10:29:22 2001 Page 19
NYC-WTC_000088930
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NYC-WTC_000087274
Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088207
Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088346
Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089418
Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088263
Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088853
Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088456
Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088556
Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088372
Laboratory report documenting GC/MS analysis of environmental sample AD23271 conducted on October 15, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089476
Laboratory report documenting GC/MS analysis of sample AD23834 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088316
Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
Filed in the same folder
NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
Filed in the same folder
NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
Filed in the same folder
NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
Filed in the same folder
NYC-WTC_000088753
Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.
Filed in the same folder