Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
NYC-WTC_000033834–000033846Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV2 601\28155.D Vial; 11 Acq On 26 Nov 2001 8:29 pm Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.
43.96 2.34 ug/1 350886 Perylene-dl2 37.11
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 38 2 1,2-Benzenedicarboxylie acid, bis(t 310 C14H2204Si2 002078-22-0 35 3 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 17 4 Pentanoic acid, 2-[(trimethylsilyl) 262 CllH2603Si2 055887-46-2 12 Abundance Scan 4239 (43.962 min): 28155. D (-) m/ z 73.00 100.00% 73 147 221 5000 281 355 "T 7 429 43.60 43.80 44.00 44.20
m/z-> 40 mfr .. .. .. 96 i" " I 19144. 2274 TH. r 40 60 80 100120140160180200220240260280300320340360380400420 401 I m/z 147.00 — 83.65% Abundance #41682:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221
73 5000 43.60 43.80 44.00 44.20
_A 191 m/z 220.9564.58% 117 279 ......... ,, .1.l... p।(1.... 1।1.... 1 T m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e 147 IT 73 43.60 43.80 44.00 44.20 5000 m/z 281.00 32.58%
m/z-> Abundance LL 45 , . ... . 119 i 193..231. 295
40 60 80 100120140160180200220240260280300320340360380400420
73 #30949: Mercaptoacetic acid, bis(trimethylsily!)-
147 . i""i ""i". 'I
"I JV 43.60 43.80 44.00 44.20 IT
m/z 354.95 22.59% 5000
m/z—> T 45 193 221
v i" " ih " r ■ "i m.. — 11।1.... 1.... 1.... 11.... । 104 40 60 80 100120140160180200220240260280300320340360380400420 7 .... ....... . 43.60 43.80 44 00 44.20
28155.D GCMS1126.M Tue Nov 27 12:58:22 2001 Page 6
NYC-WTC_000033844
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NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035700
Laboratory notes stating the GCMS scan of sample AD28901 revealed no unusual compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder