Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
NYC-WTC_000033834–000033846Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28155.D Vial: 11 Acq On : 26 Nov 2001 8:29 pm Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.
47.04 1.52 ug/1 227368 Perylene-dl2 37.11
Hit# of 5 'entative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 2 3,6-Dioxa- 2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 25 3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 4 1,3(2H/4H)-Isoquinolinedione, 6,7-d 369 C20H19NO6 000000-00-0 14 Abundance Scan 4574 (47.038 min): 28155.D (-) m/z 72.95 100.00% 73 147 221
5000 281 355 T-r-j-r-n-r-r-r 429 39 — — 119 177 4l327L +11... 1 46.80 47.00 47.20 47.40 m/z 220.95 75.55%
A. m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147
281 5000 TTT 46.80 47.00 47.20 47.40
369 m/z 147.0074.90% 207 249, — ■ — --------I 338.......... m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #41682:3,6-Dioxa-2,4,5,7-tetrasitaoctane, 2,2,4,4,5,5,7,7- 147 221 f—r ' ' I ' ‘ ' I ' ' ' 1 I ' ’ ' ' I ' ' ' 73 46.80 47.00 47.20 47.40 5000 m/z 281.00 40.53%
miz-> Abundance "Il 50
73 117
100 e 150 191
T L 200 250 279
300 350 400 #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 450 500 550 7 46'80 47.00 47'20 47.40 m/z 207.00 33.98%
5000 147 W"WwA 221 281 327 ----- — — 415 519 561 T m/z-> 50 100 150 200 250 300 350 400 450 500 550 46.80 47.00 47.20 47.40
28155.D GCMS1126.M Tue Nov 27 12:58:24 2001 Page 7
NYC-WTC_000033845
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NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035700
Laboratory notes stating the GCMS scan of sample AD28901 revealed no unusual compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder