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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004324
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************** * Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

38.02 0.45 ug/1 139789 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1, 1,1,5,5,5-hexamethyl 3 84 C12H3604Si5 003555-47-3 25 2 3,8-Dioxa-2,9/disiladecane, 2,2,9,9 234 C10H26O2Si2 018001-91-7 22 3 tert-Butylpentamethyldisiloxane 204 C9H24OSi2 067875-54-1 14 4 Ethanedioic cid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 14 Abundance Scan 3592 (38.020 min): 30709.D (-) m/ z 73.00 100.00% 73 147

5000 221 281 355

m/z-> 41 TTT -m . 95 117 193 I 327.1.. 401 429 37.60 40 60 80 100120140160180200 220240 260280 300 320 340 360380400420 37.80 38.00 38.20 38.40 m/z 147.00 67.63% Abundance #74103: Trisiloxane, 1,1,1,5,5,6-hexamethyl-3,3-bis[(trimet 73 147

5000 A-AA—AArAAF N_I_ I_ITTMM TAP 281 37.60 37.80 38.00 38.20 38.40 45 369 m/z 221.05 40.63% l , 117 207 249 T1-1—000————u9—01VuDD m/z—> 40 60 80 100120140160180200220240260280300320340360 380400420 (Abundance #71025: 3.8-Dioxa-2,9-disiladecane, 2,2.9,9-tetramethyl- 147 ...... ) V I ' 1 1 1 i ' 37.60 37.80 38.00 38.20 38.40 ■ i ' '

5000 116 m/z 207.00 23.03% 73

177 AW/WyWA/ WWA 46 219 1" ’11 I" " I ■YTpnTTTTTTTyTTTTpTTTpTTnrpTTTp^ m/z-> 40 60 80 1001201401601802002202402602803003203403 60 380400420 Abundance #23714: tert-Butyipentamethyldisiloxane i ■ ■ • • i ' 1 147 37.60 37.80 38.00 38.20 38.40 m/z 281.00 21.71% 5000 73 189 117 1 L 471 mhmmmmmmmmmmmmmm-mmmmmmmmmmmm A-AAA~N Uwyw m/z-> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 420 37.60 37.80 38.00 38.20 38.40

30709.D GCMS1126.M Mon Jan 28 11:33:45 2002 Page 15

NYC-WTC_000004324

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NYC-WTC_000004324Source: NYC Law Department, mirrored locally

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