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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004323
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 14 1,2-Benzenedicarboxylic acid, Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

36.72 0.71 ug/1 218333 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic/acid, bis(t 310 C14H22O4Si2 002078-22-0 32 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 27 3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 25 4 Propanoic acid, 2-oxo-^-(trimethyls 232 C9H20O3Si2 __ 055887-51-9 17 Abundance Scan 3450 (36.717 min): 30709.D (-) m/ z 73.00 100.00% 73

147 5000 221 281 355 36.40 36.60 36.80 37.00 327 , | 401 429 mlz-> 45 Tu*urmpnu 95 117 ...1.... 40 60 80 100120140160180200220240260280300320340360380400420 ----- odoipaanpadonuauns i,,,i।,i ,।, m/z 146.95 55.23% Abundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethylsilyi) e i U7 73 5000 36.40 36.60 36.80 37.00 45 295 m/z 221.05 34.44%

m/z-> mpp 119 193 221 TII—010—010——00133001110T17TTTjvrrrpTT-rp-rrTyTTTrrrTrrp-rTTp-rTT^^ 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74103. Trisitoxane, 1 1,1,5.5,5-pexamety-3.3-bisi{trimei 1 73 147 1 1 i r 1 p ,4 1 m 1 1 I 1 r 1 ' I 36.40 36.60 36.80 37.00 5000 m/ Z 281.00 19.97% 281 45 369 117 207 249 m/z-> Abundance 40 60 80 100120140160180200220240260280300320340360380400420 _ #71005: Ethanedioic acid, bis(trimethylsilyl) ester 73 36.40 36.60 36.80 37.00 m/z 355.05 14.67% 147 5000-

45

m/z—> massrsya ... 117 .h... 190 219 "T00——010—181017 OT1T •»< 'l1' ’' l'" T*i i I ] I I I I I : I I I I I I I J I I > I I I I I I I I I I I I I I J I I I I I I I I J 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 36.40 36.60 36.80 37.00

30709.D GCMS1126.M Mon Jan 28 11:33:41 2002 Page 14

NYC-WTC_000004323

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NYC-WTC_000004323Source: NYC Law Department, mirrored locally

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