NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47
Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
Peak Number 14 1,2-Benzenedicarboxylic acid, Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
36.72 0.71 ug/1 218333 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,2-Benzenedicarboxylic/acid, bis(t 310 C14H22O4Si2 002078-22-0 32
2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 27
3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 25
4 Propanoic acid, 2-oxo-^-(trimethyls 232 C9H20O3Si2 __ 055887-51-9 17
Abundance Scan 3450 (36.717 min): 30709.D (-) m/ z 73.00 100.00%
73
147
5000
221
281
355
36.40 36.60 36.80 37.00
327 , | 401 429
mlz->
45
Tu*urmpnu
95 117
...1....
40 60 80 100120140160180200220240260280300320340360380400420
----- odoipaanpadonuauns i,,,i।,i ,।, m/z 146.95 55.23%
Abundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethylsilyi) e
i U7
73
5000
36.40 36.60 36.80 37.00
45 295 m/z 221.05 34.44%
m/z->
mpp 119 193
221
TII—010—010——00133001110T17TTTjvrrrpTT-rp-rrTyTTTrrrTrrp-rTTp-rTT^^
40 60 80 100120140160180200220240260280300320340360380400420
Abundance #74103. Trisitoxane, 1 1,1,5.5,5-pexamety-3.3-bisi{trimei
1 73
147 1 1 i r 1 p ,4 1 m 1 1 I 1 r 1 ' I
36.40 36.60 36.80 37.00
5000 m/ Z 281.00 19.97%
281
45 369
117 207 249
m/z->
Abundance
40 60 80 100120140160180200220240260280300320340360380400420 _
#71005: Ethanedioic acid, bis(trimethylsilyl) ester
73 36.40 36.60 36.80 37.00
m/z 355.05 14.67%
147
5000-
45
m/z—>
massrsya ... 117 .h... 190 219
"T00——010—181017 OT1T •»< 'l1' ’' l'" T*i i I ] I I I I I : I I I I I I I J I I > I I I I I I I I I I I I I I J I I I I I I I I J
40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 36.40 36.60 36.80 37.00
30709.D GCMS1126.M Mon Jan 28 11:33:41 2002 Page 14
NYC-WTC_000004323
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