Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
NYC-WTC_000034180–000034197Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28263.D Vial: 33 Acq On : 29 Nov 2001 6:28 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1,2-Benzenedicarboxylic acid, Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 47.04 6.43 ug/1 953735 Perylene-dl2 37.12 Hit# of 5 Tentati ID MW MolForm CAS# Qual 1 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 22 2 Trichloromethyl 9-anthracenecarbodi 370 C16H9C13S2 091631-91-3 18 3 Trisiloxane, octamethyl- 236 C8H2402Si3 000107-51-7 14 ° 4 1,2-Bis ^brimethylsiloxy) ethane Abundance 73 Scan 4575 (47.042 min): 28263.D (-) 147 206 C8H2202Si2 m/z 007381-30-8 10 73.00 100.00% 221
5000 281 355 429 46.80 47'00 47.20 47.40 44 117 , 1911 4.234 Tm H mmm TTTTTT 401 mm | m/z 147.0088.78%
A. mlz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #72973:1 2-Benzenedicarboxylic acid, bis(trimethylsilyl) e 147
73 5000 tr 46.80 47.00 47.20 47.40
mlz-> Abundance 45 . 119 . , 193 221 TITTu —...... - TTTTTTTTTTTTTTTTTTTTT . I.......... 40 60 80 100120140160180200220240260280300320340360380400420 #51283: Tirichloromethyl 9-anthracenecarbodithioate m/z 221.05 73.75%
105 221 77 T T"" 253 46.80 47.00 47.20 47.40 5000 m/z 281.00 38.48% 177 149 TTTIITTTTTTTTTTT mmmmmp 370 T TTTTTTTTTTTTTTTTTTTTT mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280300320340 360 380 400 420 RRRRA T Abundance #30951: Trisiloxane, octamethyl- 221 46.80 47.00 47.20 47.40 m/z 354.95 29.55% 5000
m/z—> , 73
13.147 W, TTg"O"uOug"T—m"u—e—a———=p"TBTOTBTC00T000 40 60 80 100 120 140 160 180 200220 240260 280 300320 340 360 380 400 420 . A.46.80 47.00 47.20 47.40
28263.D GCMS1126.M Fri Nov 30 13:41:42 2001 Page 9
NYC-WTC_000034196
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NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035700
Laboratory notes stating the GCMS scan of sample AD28901 revealed no unusual compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder