GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30256.D Vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 1,2-Benzenedicarboxylic acid, Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

35.57 1.31 ug/1 209319 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 43 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 3 3-Isopropoxy-1, ,1/7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 4 1,2-Bis(trimeth ylsiloxy) ethane 206 C8H2202Si2 007381-30-8 23 Abundance /'Scan 3325 (35.571 min): 30256.D (-) m/z 72.95 100.00% 73 ___

147 5000 221 281 355 1"TY+18/*/tI*I**.* 3950—4100TTr 117 , 1914—— 1,4,1,4325.4, 401 4?% , 35.20 35.40 35.60 35.80 36.00 m/z 147.00 52.38% miz-> 150 200 250 300 350 400 450 500 550 Abundance #72972:1,2-Benzenedicarboxylicacid, bis(trimethylsily!) e 147

73 5000 111101 Tepe rrr 35.20 35.40 35.60 35.80 36.00 45 295 m/z 221.05 33.64% —,411944 19322- m/z-> 50 100 150 200 250 300350400450500550 Abundance #58871: 1-Monolinolecyiglycerol tmethylsilyl ether 73

35.20 35.40 35.60 35.80 36.00 207 5000 147 m/z 281.00 17.65% 34 103 281 395 482 1 ' i ■ ' ■ ■ i • ■ 1 1 r' 1 ' ■ i ' ■ ' ‘ i 1 ■ ■ ' i 1 1 ' ' i ‘ 1 ■ ' i • ■ ‘ ■ i ■ 1 • ■ i ■ 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1.1,1.7,7.7-hexamethyl-3,5,5-tris(trim MMMMMATT 73 35.20 35.40 35.60 35.80 36.00 m/z 355.05 15.26%

miz-> 5000 147

200 221 281 ■ ■ i ■ ' ' ' i 1 ■ ' ■ i • ■ ■ ■ i ■ j ' ' i ■ ■ 1 ' i ■ 50 100 150 250 300 327 — 350 415 -**/ 400 i

450 519 561 500 550 l 35.20 35.40 35.60 35.80 36.00

30256.D GCMS1126.M Wed Jan 02 10:25:12 2002 Page 14

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