NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30252.D vial: 22
Acq On : 28 Dec 2001 9:31 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 16 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 14
R.T. EstConc Area Relative to ISTD R.T.
38.02 0.90 ug/1 184431 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy- 1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 37
2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 27
3 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 17
4 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 16
Abundance Scan 3592 (38.016 min): 30252.D (-) m/ z 73.00 100.00%
73
147
5000
221
355 T ‘ I ■ ‘
39 117 191 327 [ 429 37.60 37.80 38.00 38.20 38.40
—
I* । 'i ■ • • ■ i ‘ ‘ । ■ ‘ Y. m/z 146.9 52.68%
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-trls(trim
73
5000 AMPmM
147 37.60 37.80 38.00 38.20 38.40
221 m/z 221.05 36.72%
i
i
miz-> 50 100 150 200 250
J1, 327., 415. .595
300 350 400 450 500 550
A
Abundance *71006 Ethanedioic acid, bis(trimethyleilyl) ester
73
4—T
147 37.60 37.80 38.00 38.20 38.40
5000 m/z 207.00 21.96%
45
117 190 219
vWyW "WywA
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #30949: Mercaptoacetic acid, bis(trimethylsily!)-
73 147
37.60 37.80 38.00 38.20 38.40
m/z 355.05 19.29%
5000
221
45
193
I, ,. 1 • ■ 104
■ ‘ i ' ′* ■
‘ ‘ i ' 1 ' ‘ i 1 ‘ ‘ i ‘ ■ i ■ ‘ ‘ 1 i ■ ' ‘ ‘ i ■ ' ‘ 1 I 1 1 1 1 I 1 1 I* ‘ ' I ' ‘ 1 f I 1 1 1 1 I ■ ■ i • ■
m&~> 50 100 150 200 250 300 350 400 450 500 550 37.60 37.80 38.00 38.20 38.40
30252.D GCMS1126.M Wed Jan 02 10:43:12 2002 Page 16
NYC-WTC_000017877
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