NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\30351.D Vial: 20
Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 13 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
36.71 0.48 ug/1 86792 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17
2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 16
3 2-Propenoic acid, 2-[(trimethylsily 232 C9H20O3Si2 055191-13-4 16
4 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 16
Abundance Scan 3450 (36.715 mln): 30351.D (-) m/z 73.00 100.00%
73
147
5000
221
281 355 T T T T
36.40 36.60 36.80 37.00
—
47 103
• r* ■ P
. 191. I i 327, I 429
m/z 147.00 61.65%
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503:3-lsoprapoxy-1,1,1,7,7,7-hexamethyl-3,5,5-Ws(trim
73
5000 AAMAM—P
147 36.40 36.60 36.80 37.00
221 281
m/z 221.0 35.06%
327 ... 415, 0519 561
mz—s
(Abundance
50 100 150 200 250 300 350 400 450
#71006: Ethanedioic acid, bis(trimethylsilyl) ester
500 550
t 73
147 36.40 36.60 36.80 37.00
5000 m/z 207.00 27.58%
45
117 190 219
AAA.A—wwwvAw w
' * I ' ' * * I ’ ' ‘ ‘ I ‘ ‘I 11I1*I***I‘***1***1*4/**114 ‘1—*
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #70934:2-Propenoic acid, 2-[(trimethylsilyl)oxy]-. trimeth T T T
147 36.40 36.60 36.80 37.00
73 m/z 280.95 21.26%
! 5000-
45
217
99
v—wWW V
—4 250 1 300 ‘ 350 ‘ 400 ‘ 450 ' ' 500 1 550 T T i * ‘ ‘ I
miz-> 50 100150200 36.40 36.60 36.80 37.00
30351.D GCMS1126.M Wed Jan 02 10:46:54 2002 Page 13
NYC-WTC_000017852
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