Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
NYC-WTC_000017833–000017853Folder label: “GCMS X 12/13/01 A 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30351.D Vial: 20 Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ***************************** *’* ************************************** Peak Number 12 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
35.57 1.36 ug/1 244275 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 38 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 3 3-(3-Hydroxyphenyl)-3-hydroxypropio 398 C18H34O4Si3 000000-00-0 25 4 2-Butenoic acid, 3-methyl-2-[(trime 260 CllH24O3Si2 055044-79-6 23 Abundance Scan 3325 (35.567 mln): 30351 .D (-) m/ z 73.00 100.00% 73 _
147 5000 221 281 355
m/z-> ..... Xu 240 4 44491,42, m/z 147.00 327 *411—4444—1841*8*71*4 TIMT 40 60 80 100120140160180200220240260280300320340360380400420 35.20 35.40 35.60 35.80 54.63% Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet i 73 147
5000 1—u—.—mmrovmprf 281 35.20 35.40 35.60 35.80 45 369 m/z 221.05 34.62% I , —900—00mmE—117 , 207 249 . 1101100011 IB—TT—M31 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #71006: Ethanedioic acid, bis(trimethylsily!) ester 73 1 1 t ' 147 35.20 35.40 35.60 35.80 5000 m/z 281.00 18.11% 45 i i 117 190 219 , TTTTyrtTTpTrTpTrrp-rr^ Impmgppm] miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #53668: 3-(3-Hydroxyphenyl)-3-hydroxypropionic acid, trt-TMS 73 267 35.20 35.40 35.60 35.80 ‘ * m/z 355.05 14.98% 5000 147
207 398 47 Tp[ 11," TTTTWTTTTTTTTTTTTT —I,,293 341 , L —3TI—COBU0UM0-B3T230—88307 n////Bn—nn—/n 1 1 1 1 miz-> 40 60 80 100120140160180200220240260280300320340360380400420 35.20 35.40 35.60 35.80
30351.D GCMS1126.M Wed Jan 02 10:46:50 2002 Page 12
NYC-WTC_000017851
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NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
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