NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30426.D Vial: 23
Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 14 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
36.72 0.76 ug/1 161734 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
T
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38
2 2-Methoxyphenylpyruvic acid, di-TMS 338 C16H2604Si2 000000-00-0 35
3 3-(3-Hydroxyphenyl)-3-hydroxypropio 398 C18H3404Si3 000000-00-0 32
4 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 25
Abundance Scan 3451 (36.722 min): 30426.D (-) m/z
73
147
5000
221
281 355 I* TuBnmTTTT
36.40 36.60 36.80 37.00
m/z->
42
40
"'l'"
60 80
^4142534... 327 I . 401 429
IMMgp
100120140160180200220240260280300320340360380400420
m/z 146.95 58.72%
Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73
147
5000 1 TTi TC0 . . । —DOaonorT
281 36.40 36.60 36.80 37.00
45 369 m/z 221.05 35.00%
, . 117 207 249
TU11 ,■।.. n p... 11111111 > 11 ,r, ■ ।. > 111 |"i 1111 u 111.... (. 11. ।. A . j. ।.... 11
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #,7880: 2-Methoxyphenylpyruvic act. di-TMS
147
TI T T T T
36.40 36.60 36.80 37.00
73 m/z 281.00 22.08%
5000
267
47 !____________ ! 207 1 307
. ■. J,... I. ■ ■ ■ 11 > > ■ J11 ■ >! 11.1 j ■ 11 > > !■■•■i■■' ‘ I pT-irp+TTjTTTTp-rrry J.........।..111....11... 11
m/z-> 40 60 80 100120140160180200220240260280300320340360380406420
Abundance #53668:3-(3-Hydroxyphenyi)-3-hydroxypropionic acid, tri-TMS
i
73 267 36.40 36.60 36.80 37.00
! m/z 355.05 17.39%
5000 147
207 398
47
miz-s
mmmt
mp TI । i < > i । > i > > । t i i i । r 11 i j r i > i । 11 > > । i i i i । t i i i । i i i i । I 1293
40 60 80 100120140160180200220240260280300320340 360380400420
341
T
..
j » I I i I 7 r » » I I I r . ]
36.40 36.60 36.80 37.00
30426.D GCMS1126.M Wed Jan 02 11:08:38 2002 Page 14
NYC-WTC_000017745
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