DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30650.D Vial: 46 Acq On : 30 Dec 2001 3:26 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

35.57 0.90 ug/1 247231 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5/5,5-hexamethyl 384 C12H3604Si5 003555-47-3 43 2 Ethanedioic acid, s(trimethylsily 234 C8H1804Si2 018294-04-7 35 3 1,2-Bis(trimethyl iloxy)ethane 206 C8H2202Si2 007381-30-8 25 4 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 __ 002078-22-0 23 Abundance Scan 3325 (35,570 min): 30650.D (-) 73 m/ z ~ 73 TT " 147 5000 221 281 2EE . , । . ri , । rn ■' । । । । । । । 55 . 96 117 , 191 1 i 2511.. .......... . । 1 , ,V| ,,,, ।।, ii i 11 ■ । iTi. ।.. TTMTTT1011011111101101—0110-10110111110101010103011317017 35.20 35.40 35.60 35.80 36.00 m/z 147.00 54.91% m/z-> 40 60 80 100120140160180 200220240260 280300 320 340 360 380400420 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyi-3,3-bis[(trimet 73 147

5000 —------ 281 35.20 35.40 35.60 35.80 36.00 45 369 m/z 221.05 30.32% I 117 207 249 1 1" 111" I" " I'11' I" " i ■ ■" i' " r "' i" " i" " i" " i"' ■ i' ■" P1111. ।< 11. ■ 11. <. ■ । < ii. 11.111 < > 1111 < 111 > m/z-> 40 60 80 100120140160180 200220 240260 280 300 320 340 360 380400420 Abundance *71006 Ethanedioic acid, bisit imotty si! 7i: oster 1 73 ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ 147 35.20 35.40 35.60 35.80 36.00 5000 m/z 281.00 19.50 45 117 190 219 m/z-> 40 60 80 100120140160180 200220240 260 280 300 320 340 360 380400420 Abundance #70005:1,2-Bis(trimethylsiloxy)ethane 147 aPRRRe 1 ' i 1 35.20 35.40 35.60 35.80 36.00 m/z 207.00 14.97% 73 5000

191 47 [.......................................................... ’ 01’1111111111101110111000113301103311101030101—090—0001081317 m/z-> 40 60 80 100120140160180 200220240 260 280 300 320 340 360 380 400 420 35.20 35.40 35.60 35.80 36.00

30650.D GCMS1126.M Mon Jan 28 11:19:02 2002 Page 14

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