NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30352.D Vial: 19
Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
35.58 2.21 ug/1 453260 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 35
2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 25
3 Propanoic acid, 2-oxo-3-(trimethyls 232 C9H20O3Si2 055887-51-9 25
4 Propanedioic acid, bis(trimethylsil 248 C9H20O4Si2 018457-04-0 17
Abundance Scan 3326 (35.575 min): 30352.D (-) m/z 73.00 100.00%
73
147
5000
221
185 281
1
43 ,
442,1,4217*81 "II 166 ... ....................................
355
..................... 401429 35.20 35.40 35.60 35.80 36.00
TTTOTPnnf mm m/z 147.00 54.57%
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis((trimet
73
147
5000 r l r • > • | i ' 1 । | i । । i|T > I i" । "i1
281 35.20 35.40 35.60 35.80 36.00
45 369 m/z 221.05 32.58%
I 019011903118837183
, I 207
117 TII9n—89mmBppumm 249 . L________________1_____________
$— TTTTpTTTpTTTyTTTTp-ftT^^
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #71006. Ethanedioic acid, bis(trimethylsilyl) ester
73
147 35.20 35.40 35.60 35.80 36.00
5000 m/z 185.10 21.43%
45
117 190 219
TTTTpTTTpTTTpTTTpTT^ T l ahut j i I ppi i *. 1.».»J». 111.. I. |. 11. ] I.. H . I» 4 m . i [m 11 H J J111 H JIJ U 11
miz-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #30222: Propanoic acid, 2-oxo-3-(trimethylsilyl)-, trimethy
147 35.20 35.40 35.60 35.80 36.00
73 m/z 281.00 18.73%
5000
45
217
. ............................................................................................................................
m/z-> 40 60 80 100 120140160180 200 220 240 260i 280 300 320 340 360 380 400 420 ' 35.20 35.40 35*60 35.80 36.00
30352.D GCMS1126.M Wed Jan 02 10:51:17 2002 Page 15
NYC-WTC_000017830
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