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GCMS analysis results for sample AD30352, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.

NYC-WTC_000017808–000017832

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017831
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30352.D Vial: 19 Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 3-(3-Hydroxyphenyl)-3-hydroxyp Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

36.72 0.79 ug/1 162894 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(3-Hydroxyphenyl)-3-hydroxypropio 398 C18H3404Si3 000000-00-0 25 2 1,2-Bis (trimethylsiloxy) ethane 206 C8H2202Si2 007381-30-8 16 3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 16 4 2-Methoxyphenylpyruvic acid, di-TMS 338 C16H2604Si2 000000-00-0 16 Abundance Scan 3451 (36.723 min): 30352.D (-) m/z 73.00 100.00% 73

147 5000 221 281 355 36.40 36.60 36.80 '37'00 ‘ Tp 193...— 253A.47 325. ...... 401429 47 105 ,,.. I,, .T| > ri 111111 fi 111 irrtrf rn/z 147.00 56.75% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #53668:3-(3-Hydroxyphenyl)-3-hydroxypropionic acid, tri-TMS 73 267

5000 147 36.40 36.60 36.80 37.00 207 398 m/z 221.05 38.12% 47 I | 293 341 T01mmmnnp"anpmpppunuDaTg wepuu"n" “uumn—Dmm miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #70005: 1 2-Eis(trimethvisiloxy)ethane 147 ‘ ■ I ‘ ‘ 1 ‘ I ' ‘ ' I ' ' r ‘ I TOI 36.40 36.60 36.80 37.00 73 5000 m/z 281.00 20.47% 103 191 .7. ;.......... .... ... .... miz-> ‘ 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400420 " ‘ Abundance #71005: Ethanedioic add, bis(trimethylsily!) ester T T T T T 73 36.40 36.60 36.80 37.00 m/z 207.00 18.78% 147 5000 soour/ o 45

miz-> ‘ 1 mm 117 190 219 111 “11 '’U1 TIDgmmpT 40 60 80 100120140160180200220240260280300320340360380400420 TTnr T T T 36.40 36.60 36.80 37.00

30352.D GCMS1126.M Wed Jan 02 10:51:21 2002 Page 16

NYC-WTC_000017831

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NYC-WTC_000017831Source: NYC Law Department, mirrored locally

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