GCMS calibration table with surrogate recovery data, Feb 16, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1502\1137.D Vial: 10 Acq On : 16 Feb 2002 12:12 am Operator: 209 GALOS Sample : gc/ms scan 1/16 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-(3-Hydroxyphenyl)-3-hydroxyp Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

36.23 0.41 ug/1 46769 Perylene-dl2 38.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(3-Hydroxypheny) -3-hydroxypropio 398 C18H3404Si3 000000-00-0 33 2 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 32 3 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 30 4 3-1sopropoxy-1, ,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 Abundance Scan 3398 (36.235 min): 1137.D (-) m/ Z 73.00 1 00.00% 73

147 5000 221 1 281 355 ‘IT T T VTT 44 ,k 191 [ [ Y 429 36.00 36.20 36.40 36.60

m/z-> m/z " 61.68% 50 100 150 200 250 300 350 400 450 Abundance #53668: 3-(3-Hydroxyphenyl)-3-hydroxypropionlc acid, tri-TMS 73 267

A N 5000 147 ‘ 1 i ■ ‘ ■ ' f • • • ■ i ‘ ■ 36.00 36.20 36.40 36.60 207 398 m/z 221.05 34.54% 47 ———————— 111293.7 T 341 m/z->__ 50____ 100 ___ 150___ 200 250 300 350 400 450 Abundance ta A J’oreptlr efin d. WBimil*eShvir 73 147 1*1* ■ ■ i • ■ 36.00 36.20 36.40 36.60 5000 rn/z 207.00 20.41% 45 104 193 221 AAP"wl m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73 36.00 36.20 36.40 36.60 m/z 281.00 18.54% 207 5000 147 34 103 281 li.............. 395 ............ 482 Wpna WyA ■ ' i ■ ’ ‘ ‘ ' I ‘ ‘ ' i 1 ‘ ■ i • ■ ' ■ I 1 1 1 ' m/z-> 50 100 150 200 250 300 350 400 450 _ 38.00 36.20 36.40 36.60

1137.D GCMS0208.M Mon Mar 04 15:09:50 2002 Page 2

NYC-WTC_000009635