Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018492–000018518Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\28322.D vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
35.57 2.50 ug/1 600692 Perylene-d12 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 3 9,12,15-Octadecatrienoic acid, 2,3- 496 C27H5204Si2 055521-22-7 23 4 l,l,l,3,5,5,7,7,7-Nonamethyl-3-(tri 384 C12H3604Si5 038146-99-5 23 Abundance Scan 3325 (35.569 min): 28322.D (-) m/z 73.00 1 00.00% 73
147 5000 221 281 355 ~' i ■ ■ ■ ‘ i ‘ ‘ ■ i ' ‘ i ■ ■ ‘ • i ‘ 35.20 35.40 35.60 35.80
miz-> 45 ■ r’T r 50 117 100 4.11914., 2404 14327/ 1,.4014?%. . 150 200 250 300 350 400 450 500 550 m/z 147.00 49.92% Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3.5,5-tris(trim 73 ■| l ■ ■ r i | । । < i 11- 5000 -r-T-r-r 147 35.20 35.40 35.60 35.80 m/z 221.05 32.71%
X 221 281 327 415 ------ l 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 710 ' thanedolc atu, bisftrimniathyisily") ester 73 ■ ■ i • 147 35.20 35.40 35.60 35.80 5000 m/z 281.00 18.39% 45 117 190 219 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance "'#58836:9,12,15-Octadecatrienoicacid, 2,3-bis[(trimethyisi MMP ■ • T > ■ ■ ■ i ■ • ■ । । । । | । 73 35.20 35.40 35.60 35.80 147 m/z 355.05 14.80% 220 5000 109 191 281 249 377 1 i 1 117 '"r /, Y i । i । > i । । , 711, | I 452 m/z-> 50 100 150 200 250 300 350 400 450 500 550 35.20 35.40 35.60 35.80
28322.D GCMS1126.M Wed Feb 06 12:56:56 2002 Page 17
NYC-WTC_000018514
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NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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