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GC/MS calibration data for sample 28322, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018492–000018518

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Ethanedioic acid, bis(trimethy Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

34.38 2.52 ug/1 846555 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 2 Propanoic acid, 2-oxo-3-(trimethyls 232 C9H20O3Si2 055887-51-9 32 3 N-Benzhydrylidene-1-(2,4,6-trimethy 343 C24H25NO 089839-57-6 27 4 1,2-Bis(trimethylsiloxy)ethane 206 C8H2202Si2 007381-30-8 23 Abundance Scan 3195 (34.376 min): 28322.D (-) m/ z 73.00 100.00% 73

147 5000 221 281 355 1 1 1 ' ■n-p-r-n-p- 34.00 34.20 34.40 34.60 34.80

m/z-> « 45 , 96 117 , 0-m 11r ।»11111;/|।i»i।a>J. 1914. 249 „ 1 t 327 TTAMTMDTTT Trmm TWMmp] 40 60 80 100120140160180200220240260280300320340360380400420 401 42% m/z 147.00 50.45% Abundance #71005: Ethanedioic acid, bis(trimethylsily!) ester 73 147 5000 --r । r 11. , ■ r 1 ' I 1 1 1 1 I 1 34.00 34.20 34.40 34.60 34.80 45 m/z 221.05 29.95% I . I 117 190 219 ““i ""i" 11 • • ■ • i ■ “ ■ i ■ Tpmpmmp m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #30222: Propanoic acid 2-xo-3-tldmethyisilyh)- nmethy 147 73 1 i 1 ‘ ' 1 i 1 34.00 34.20 34.40 34.60 34.80 5000 m/z 281.0.0 17.13% 45 • 217 117 | 189 ।।।।। ।11।r ।।।. I n 111111 u 111 u 111111111 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48514: N-Benzhydrylidene-1-(2.4,6-trimethylphenyl)ethylami ..... 147 34.00 34.20 34.40 34.60 34.80 m/z 355.0.5 15.98% 5000

165 , 197 312 343 Dppy TTffrrriVrrTpTTTpTTTpTTTpTTTpTTTpTTTprrrp^ T-p-n-p-r miz-> 40 60 80 100120140160180200220240260280 300320340360380400420 34.00 34.20 34.40 34.60 34.80

28322.D GCMS1126.M Wed Feb 06 12:56:52 2002 Page 16

NYC-WTC_000018513

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NYC-WTC_000018513Source: NYC Law Department, mirrored locally

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