Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018519–000018545Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Ethanedioic acid, bis(trimethy Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.
33.08 7.42 ug/1 2605750 Chrysene-dl 2 33.02
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 38 2 l,l,l,3,5,5>;7,7-Nonamethyl-3-(tri 384 C12H36O4Si5 038146-99-5 23 3 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 4 9,12,15^0 adecatrienoic acid, 2,3- 496 C27H52O4Si2 055521-22-7 23 Abundance Scan 3054 (33.084 mln): 28323.D (-) m/z 73.00 100.00% 73
5000 147 221 281 355 ■ 1 i ■ • ■ U I • ' ‘ • i ' ' 249 , . 309327 . 383401 429 32.80 33.00 33.20 33.40 45 96 117 ,*...... 0- TmITpmm m/z 147.00 47.35%
k miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #71005: Ethanedioic acid, bis(trimethylsilyl) ester 73
147 5000 TT-j-r-T 32.80 33.00 33.20 33.40 45 m/z 221.05 28.97%
m/z-> mpm 117 —011—817 190 219 40 60 80 100120140160180200220240260280300320340360380400420 Abundance 240. - ■ .3,5 5 777Moname timgthylsiloxy)tet 73 11/3.8 281 32.80 33.00 33.20 33.40 5000 147 m/z 355.05 18.69% 369 45 207 m/z-> 40 60 80 100 120 146 160 180 200 220240 260 280 300 320 340 360 380 400 420 " Abundance #71782: Butanoic acid, 3-methyl-2-[(trimethylsilyl)oxy]- t ' ' 1 1 ' ' ' 1 l-1 ' 1 ' I 1 1 73 32.80 33.00 33.20 33.40 145 m/z 281.00 17.87% 5000
45 190 219 247 mpmTIWgTT | 117 TTmnmpmmup m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 32.80 33.00 33.20 33.40
28323.D GCMS1126.M Wed Feb 06 13:02:31 2002 Page 15
NYC-WTC_000018539
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018416
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NYC-WTC_000018417
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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