NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30351.D Vial: 20
Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 11 Ethanedioic acid, bis(trimethy Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
34.37 1.27 ug/1 308833 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32
2 3-Isopropoxy-1,1,1,7,7,7 -hexamethyl 576 C18H5207Si7 071579-69-6 25
3 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23
4 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23
Abundance Scan 3195 (34.374 min): 30351.D (-) m/ z 73.00 100.00%
73
5000 147
221
281 355 • I 1 *
40
TTIT W-r —1931——251.43274
117 401 4? 34.00 34.20 34.40 34.60 34.80
m/z 147.00 47.18%
m/z-> 50 100 150 200 250 300 350 400 450 500 550 .............
Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester
73
147
5000
34.00 34.20 34.40 34.60 34.80
45 m/z 221.05 27.66%
I, I 117 .
1 ‘I ‘ ' • 4 i ■ ■ i ■ i ■
190 219 .......
m/z-> 50 100 150 ‘ 200 250 300 350 400 450 500 550
Abundance #60503: 3-Isopropoxy1.1 1.7 7.7-hexametnyl-3,5,5-tris(trim
73
I
34.00 34.20 34.40 34.60 34.80
5000 m/z 281.00 14.79%
147
221 281
327 .......... 415 ........ 519 561
■ ■ i • ' ■ ■ i ■ ■ ■ ■ I ■ ■ ‘ ■ i ' ■ ■ ■ i ■ ■ 1 ■ i ■
miz-> 50 100 150 200 250 300 350 400 450 500 SSO
Abundance #40777:2-Hexenediolc acid, bis(trimethylsilyl) ester, (E)- A.1.M444.TPRWM
73 34.00 34.20 34.40 34.60 34.80
m/z 355.05 14.28%
5000
miz->
45
' '1* ‘
50
112
147
244 273
100 150 200 250 300 350 400 450 500 ’ 550
A
34.00 34.20 34.40 34.60 34.80
30351.D GCMS1126.M Wed Jan 02 10:46:45 2002 Page 11
NYC-WTC_000017850
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