NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\30351.D Vial: 20
Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 10 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
31.71 1.94 ug/1 472226 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 43
2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40
3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5S16 038147-00-1 12
4 Prost-13-en-l-oic acid, 9-(methoxyi 599 C30H61NO5Si3 072150-30-2 10
Abundance Scan 2905 (31.712 min): 30351 .D (-) m/z 73.0.0 100.00%
73
5000 147
221 I » I l i » i I 1 I . I I « i 11 gi 11* I
281 31.40 31.60 31.80 32.00
45 117 , 1914. —— 251.4 1 + 1* i T" V । । ri । । ।327.355 401 ^29
miz->
■ ' •I 1 1
50
If
100 150 200 250 300 350 400 450 500
।
550
. m/z 147.00 37.92%
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 147
281
5000
1 1 1 1 ' ---PP 300 338350 4 .....
207 249
369 m/z 731.40 31.60 31.80 32.00
21.91%
m/z-> 50 100 150 400 450 500 550
200 250
Abundance #60503; 3-Isopropoxy-1,1.1.7.7.7-hexamethyl-3.5.5-tris(trim
73
1 1 1 1 1 1 1' I ’ 1 > ' 1 "T ' ' ■ • i ■ • • ■ i
31.40 31.60 31.80 32.00
5000- m/z 281.00 14.12%
147
221 281 327
415
i 519 561
■ ■ I ‘ ■
m/z-> 1 50 100 ' 150 1 ' 200 ' 250 300 350 400 450 500 550
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t *I**S‘‘‘II * * i > * < * ।
73 31.40 31.60 31.80 32.00
m/z 355.0 9.97%
147
I 5000 267
355 429
45 207
■ ■ i **1*114 r”' IIIFII [3T ’ I • • « f | » 1 ’ ‘ | ’ T-Yn-rn-r-j-r-r-r-r-p-r-r r-i-j-i » i J | » ‘ ‘ t ‘ ‘ ‘ I
miz-> 50 100 150 200 250 300 350 400 450 500 550 31.40 31.60 31.80 32.00
30351.D GCMS1126.M Wed Jan 02 10:46:39 2002 Page 10
NYC-WTC_000017849
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