GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30256.D Vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

34.38 1.15 ug/1 307994 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1/1,7,7,7-hexamethyl 576 C18H52O7S17 071579-69-6 40 2 Trisiloxane, 1, 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 3 1,1,1,3,5,5,7,7 ,7-Nonamethyl-3-(tri 384 C12H36O4S15 038146-99-5 23 4 2-Hexenedioic a cid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 Abundance Scan 3195 (34.377 min): 30256.D (-) m/z 73.00 100.00% 73

5000 147 221 -------------------- 281 355 , [ , 327, [ 401 429 34.00 34.20 34.40 34.60 34.80 1 45 117 , , 191 1

.1 ■ /'i 1 r 1 *i • ■ • 4/3 4 i । h*ia .1,11 . 11* r < । . । i < । . > < । । i m/z 147.00 47.70% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 —। । « » । » । t » / » । । , r fTer in 147 34,00 34.20 34.40 34.60 34.80 221 281 A4E m/z 221.05 28.34% ............... . ...................... ............. 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 ’ 550 Abundance #74103. Trisiloxane, 1,1.1 5.5,5-hexamethyl-3,3-bisi(tiimet 73 147 ■ i ' ■ ‘ ■ i • ■ l ■ 34.00 34.20 34.40 34.60 34.80 5000 m/z 281.00 18.46% 281 45 369 117 207 249 | /1+**JSI1I[11V|V miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52460:1.1.1.3.5.5,7.7.7-Nonamethyl-3-(trimethylsiIoxy)tet 1794 PAAPA. । ==ry==p*= 73 34.00 34.20 34.40 34.60 34.80 m/z 355.05 16.00% 281 5000 147 369 207 45 | ■ >•1 * 1 • • i ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 34.00 34.20 34.40 34.60 34.80

30256.D GCMS1126.M Wed Jan 02 10:25:07 2002 Page 13

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