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GC/MS calibration data for sample 28323, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018519–000018545

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018538
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 3-Isopropoxy- 1,1,1,7,7,7-hexam Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

31.72 6.30 ug/1 2211970 Chrysene-dl2 33.02

Hit# of 5 Tentative 1 MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1.7, 7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 2 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 32 3 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 4 2-Hexenedio>c acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 Abundance Scan 2905 (31,717 min): 28323.D (-) m/ z 73.00 100.00% 73

5000 147 221 281 355 31.40 31.60 31iso' 32.00 ‘ ‘ 1 249, 401 429 45 ■ rtr 117..4 . , 1911 k । । 1* Fih । ri ri”L t —trt . 327, | l I I ■ | I , . ! | . m/z 147.00 42.85% miz-> 50 100 150 200 250 300 400 350 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 31.40 31.60 31.80 32.00 221 281 m/z 221.05 25.29% 327 415 519 561 *r1//*/*1/**/1/*1////2/*/1//n////2//"/".I — • • । • • • > । L • i •n . . j i . miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71006 Ethana lioc acc, istimethyisilyi) ester 73

147 31.40 31.60 31.80 32.00 ‘ 5000 m/z 281.00 17.45% 45 117 190 219 miz-> ‘50 100 150 200 “ 250 300 350 400 450 500 550 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet ■ ■ i■ ■ ■ ■ i ■• • -T1 ■ ‘■ i ‘ ■ ■ ■i 73 31.40 31.60 31.80 32.00 147 rn/z 355.05 13.08% 5000 281 45 369 — 117 ( , 207 , 249, m/z- 50 100 150 200 250 300 350 400 450 500 550 3140 31.60 31.80 32*00

28323.D GCMS1126.M Wed Feb 06 13:02:26 2002 Page 14

NYC-WTC_000018538

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NYC-WTC_000018538Source: NYC Law Department, mirrored locally

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