Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
NYC-WTC_000017854–000017878Folder label: “GCMS X 12/13/01 A 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30252.D Vial: 22 Acq On : 28 Dec 2001 9:31 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
31.72 3.50 ug/1 958031 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 3 2-Hexenedioic acid, bis(trimethylsi 288 C12H24O4Si2 055494-10-5 23 4 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 Abundance Scan 2906 (31.719 min): 30252.D (-) m/z 73.00 100.00% 73
5000 147 221 i i । i an । » j » t i » » । « » j 281 31.40 31.60 31.80 32.00
miz-> 45 1111 r ,-117,4 .11914,, 50 100 150 200 250 24944 327,315, ...... . 300 350 400 450 500 550 m/z 147.00 41.67% Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 147 3140 31.60 31.80 32.00 ' ' m/z 221.05 24.65% 221 281 327 415 i 519 561 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71006: Ethanedioic add, bis(trimethylsilyl) ester 73 011 NT ... 147 31.40 31.60 31.80 32.00 5000 m/z 281.00 16.14% 45 117 { 190 219 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40777:2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- 73 31.40 31.60 31.80 32.00 1 m/z 355.05 12.15% 5000 147 45
I 112 ■ -T* 1 ' ■ i • 244 273 ______________________ _________ 1 ‘ I ‘ ‘ ‘ I ‘ • • I ‘ ‘ ‘ I mz-> 50 100 150 200 250 ' 300 350 400 ' 450 " 500 550 31,40 31,60 31.80 32,00
30252.D GCMS1126.M Wed Jan 02 10:42:50 2002 Page 11
NYC-WTC_000017872
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NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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