DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D vial: 14 Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

32.41 0.50 ug/1 198343 Chrysene-dl2 33.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual --- /--------- 1 3-Isopropoxy-1/1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Butanoic acid/ 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 23 4 Trisiloxane J 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 12 Abundance 7.... Scan 2981 (32.407 min): 30648.D () -..... ..................... 73.00. 100.00% m/ z 73

5000 147

221 231 3= 32.00 32.20 32.40 32.60 32.80 45 117. . 1911 249., 1 , 3272 401 429 ' ''r1 r ■ ■ । . । . - m/z 147.0,0 43.80% mlz-2. 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 ■ i ■ ■ 147 32.00 32.20 32.40 32.60 32.80 m/ z 221.05 21.58% | 3f29 I....... 281 ........................... 221 jc 7......... 415........... 519 561 m/z->50 100 150 200 250 300 350 400 450 500 550 Abundance - . 73 145 32.00 32.20 32.40 32.60 32.80 5000 m/ z 2 81.00 15.87% 45 117 190 219 24 7 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester ■ ■ i 1 ' 713 147 32.00 32.20 32.40 32.60 32.80 m/ Z 2 07.00 10.61% 5000 45

,J , TTTT 190 219 .... m/z-> 50 100 150 200 250 300 350 400 450 500 550 32.00 32.20 32.40 32.60 32.80

30648.D GCMS0103.M Thu Feb 14 11:02:15 2002 Page 13

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