DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D Vial: 14 Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

30.94 0.55 ug/1 217466 Chrys ene-d12 33.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 38 2 3-Isopropoxy/l,1,1,7,7,7-hexamethyl 576 C18H5207S17 071579-69-6 33 3 Prost-13-en/l-oic acid, 9-(methoxyi 599 C30H61NO5Si3 072150-30-2 17 4 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 17 Abundance Scan 2821 (30.938 min): 30648.D (-) m/ Z 73.00 100.00% 73

5000 147 221 281 355 30.60 30.80 31.00 31.20 45 117 , 1911 . 249., L ,327, 1, 401 429 m/z 147.00 36.82% m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73

147 - 5000 267 355 429 30.60 30.80 31.00 31.20 45 207 m/z 221.05 18.02%

m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance 73 .............................. ......... 30.60 30.80 31.00 31.20 5000 m/ z 281.00 13.01% 147 221 281 327 415 519 561 m/z-> ____ 50 100 150__ 200 250__ 300 350__ 400 450__ 500 550__ 600 Abundance #74727: Prost-13-en-1 -oic acid, 9-(methoxyimino)-11,15-bis[ - 7|3 30.60 30.80 31.00 31.20 m/z 355.05 11.39% 5000

133 355 426 47 • ■ i > ■ 1111144, 186 225 ' i ■ ■ ‘ ‘ i ‘ 327 J ' i ■ ' ■ ■ i ‘ ‘ 1 , 528 ' i ' ' ‘ ' i ■ ' ' 1 i ' ' 584 m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 30.60 30.80 31.00 31.20

30648.D GCMS0103.M Thu Feb 14 11:02:11 2002 Page 12

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